Mettler Toledo pH ISM Qualificaction Kit Mode d'emploi

pH ISM Qualification Kit

Instruction manual

Bedienungsanleitung

Instructions d’utilisation

1258

pH ISM Qualification Kit

52 300 439 E

pH ISM Qualification Kit © 12/2018 Mettler-Toledo GmbH, Greifensee

52 300 439 E Printed in Switzerland

2 pH ISM Qualification Kit

English Page 3

Deutsch Seite 25

Français Page 47

Printed in Switzerland 52 300 439 E

pH ISM Qualification Kit 3

pH ISM Qualification Kit

Instruction manual

Bedienungsanleitung

Instructions d’utilisation

pH ISM Qualification Kit © 12/2018 Mettler-Toledo GmbH, Greifensee

52 300 439 E Printed in Switzerland

4 pH ISM Qualification Kit

1 Safety.........................................................................................5

2 Important notes...........................................................................6

2.1 Notes on operating instructions .............................................6

2.2 Intended use .......................................................................6

2.3 Safety instructions................................................................7

2.4 Correct disposal of the simulator............................................9

2.5 Examples of some typical applications...................................9

2.6 Use in Ex-zones ................................................................10

2.7 Ex-classification ATEX .......................................................10

2.7.1 Introduction ...........................................................10

2.7.2 Rated data.............................................................11

2.7.3 Special conditions ..................................................12

2.8 Ex-classification FM approved ............................................13

2.8.1 Introduction ...........................................................13

2.8.2 Rated data ............................................................14

2.8.3 Special conditions ..................................................14

2.8.4 Applied Standards ..................................................15

3 Product Description ...................................................................16

4 Operation..................................................................................17

4.1 Connecting the transmitter to the pH ISM Qualification Kit .......17

5 Product Specification.................................................................19

5.1 Simulator, Pre-registered Values ..........................................19

5.2 Sensor Wear Data..............................................................19

5.3 Warnings and Alarms.........................................................20

6 Installation................................................................................21

6.1 Dimensions ......................................................................21

7 Ordering Information .................................................................22

8 Protocol....................................................................................23

Contents

Page

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pH ISM Qualification Kit 5

1 Safety

This instruction manual lists the main points of how to use the

pH ISM Qualification Kit from METTLER TOLEDO for best results

and in the intended manner.

This instruction manual, and the safety requirements in particular,

must be observed by the operator and all other persons working

with this equipment.

The instruction manual must always be stored close at hand, in a

place accessible to all people working with an ISM pH sensor and

the pH ISM Qualification Kit.

Warning notices and symbols

This instruction manual identifies safety instructions and additional

information by means of the following symbols:

This symbol draws attention to safety instructions and warnings of

potential danger which, if neglected, could result in injury to persons

and/or damage to property.

This symbol identifies additional information and instructions

which, if neglected, could lead to defects, inefficient operation and

possible loss of product.

pH ISM Qualification Kit © 12/2018 Mettler-Toledo GmbH, Greifensee

52 300 439 E Printed in Switzerland

6 pH ISM Qualification Kit

2 Important notes

2.1 Notes on operating instructions

These operating instructions contain all the information needed for

safe and proper use of the pH ISM Qualification Kit.

The operating instructions are intended for personnel entrusted with

the operation and maintenance of the sensors. It is assumed that

these persons are familiar with the equipment in which the sensor is

installed.

Warning notices and symbols

This instruction manual identifies safety instructions and additional

information by means of the following symbols:

This symbol draws attention to safety instructions and warnings of

potential danger which, if neglected, could result in injury to persons

and/or damage to property.

This symbol identifies additional information and instructions

which, if neglected, could lead to defects, inefficient operation and

possible loss of production.

2.2 Intended use

The METTLER TOLEDO pH ISM Qualification Kit is intended solely

for the qualification of pH measuring systems as described in

this instruction manual.

Any use of this kit which differs from or exceeds the scope of use de-

scribed in this instruction manual will be regarded as inappropriate

and incompatible with the intended purpose.

The manufacturer/supplier accepts no responsibility whatsoever for

any damage resulting from such improper use. The risk is borne

entirely by the user/operator.

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pH ISM Qualification Kit 7

Other prerequisites for appropriate use include:

– Compliance with the instructions, notes and requirements set out

in this instruction manual.

– Acceptance of responsibility for regular inspection, maintenance

and functional testing of all associated components, also includ-

ing compliance with local operational and plant safety

regulations.

– Compliance with all information and warnings given in the

documentation relating to the products used in conjunction with

the sensor (housings, transmitters, etc.).

– Observance of all safety regulations governing the equipment in

which the sensor is installed.

– Correct equipment operation in conformance with the prescribed

environmental and operational conditions, and admissible

installation positions.

– Consultation with METTLER TOLEDO Process Analytics in the

event of any uncertainties.

2.3 Safety instructions

– The plant operator must be fully aware of the potential risks and

hazards attached to operation of the particular process or plant.

The operator is responsible for correct training of the workforce,

for signs and markings indicating sources of possible danger,

and for the selection of appropriate, state-of-the-art instrumen -

tation.

– It is essential that personnel involved in the commissioning,

operation or maintenance of these simulators or of any of the

associated equipment (e.g. housings, transmitters, etc.) be

properly trained in the process itself, as well as in the use and

handling of the associated equipment. This includes having

read and understood this instruction manual.

pH ISM Qualification Kit © 12/2018 Mettler-Toledo GmbH, Greifensee

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8 pH ISM Qualification Kit

– The safety of personnel as well as of the plant itself is ultimately

the responsibility of the plant opera- tor. This applies in particular

in the case of plants operating in hazardous zones.

– The pH sensor simulators and associated components have no

effect on the process itself and cannot influence it in the sense of

any form of control system.

– Where specific safeguards such as locks, labels, or redundant

measuring systems are necessary, these must be provided by the

plant operator.

– A defective simulator must neither be installed nor put into service.

– No modifications to the simulators and the accessories are

allowed. The manufacturer accepts no responsibility for damages

caused by unauthorized modifications. The risk is borne entirely

by the user.

– When using cables for simulator connection not supplied and

recommended by the manufacturer the following standards need

to be considered:

• US National Electrical Code

®

(ANSI/NFPA 70 [NEC

®

]),

where applicable.

• Canadian Electrical (CE) Code

®

(CEC Part 1,

CAN/CSA-C22.1), where applicable.

– For guidance on US installations, see ANSI/ISA-RP12.06.01,

Installation of Intrinsically Safe Systems for Hazardous (Classi-

fied) Locations.

– Control room equipment connected to intrinsically safe associated

apparatus in the US should not use or generate more than the

specified Um of the associated apparatus.

– Care must be taken during installation to avoid impacts or friction

that could create an ignition source.

– Tampering and replacement with non-factory components may

adversely affect the safe use of the system.

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pH ISM Qualification Kit 9

– Insertion or withdrawal of removable electrical connectors or

modules is to be accomplished only when the area is known to

be free of flammable vapors.

– WARNING ! INTRINSICALLY SAFE APPARATUS CAN BE A

SOURCE OF IGNITION IF INTERNAL SPACINGS

ARE SHORTED OR CONNECTIONS OPENED.

– WARNING ! DO NOT OPEN WHEN AN EXPLOSIVE ATMOSPHERE

IS PRESENT.

– WARNING ! SUBSTITUTION OF COMPONENTS MAY IMPAIR

INTRINSIC SAFETY.

– WARNING ! SUBSTITUTION OF COMPONENTS MAY IMPAIR

SUITABILITY OF THE EQUIPMENT.

– WARNING ! FOR CONNECTION ONLY TO NON-FLAMMABLE

PROCESSES.

– WARNING ! TO MAINTAIN THE ENCLOSURE IP66 RATING,

THE CONNECTOR MUST BE FULLY ENGAGED.

2.4 Correct disposal of the simulator

When the simulator is finally removed from service, observe all local

environmental regulations for proper disposal.

2.5 Examples of some typical applications

Below is a list of examples of typical fields of application for the pH

sensor simulators. This list is not exhaustive:

– Tool for qualification of pH measuring systems

– Service tool for quick checks and loop troubleshooting

pH ISM Qualification Kit © 12/2018 Mettler-Toledo GmbH, Greifensee

52 300 439 E Printed in Switzerland

10 pH ISM Qualification Kit

2.6 Use in Ex-zones

Attention!

For an installation in Ex-zones please read the guidelines following

hereafter:

1258

Ex-classification ATEX

Ex ia IIC T6/T5/T4/T3 Ga/Gb

Number of the test certificate:

SEV 14 ATEX 0168X

IECEX SEV 14.0025X

Ex-classification FM approved:

IS/I,II,III/1/ABCDEFG/T6 Ta = 60 ºC

- 53 800 002; Entity

Project ID: 3021227

FM certificate number: FM16US0034X

FM18CA0021X

2.7 Ex-classification ATEX

2.7.1 Introduction

According to Directive 2014/34/EU (ATEX 95) Appendix l, pH ISM

sensor simulators are devices group ll, category 1/2G and according

to RL 99/92/EG (ATEX 137) may be used in zones 0/1 or 1/2 or

1 or 2 and gas groups llA, llB and llC that are potentially explosive

due to combustible substances in above stated temperature classes.

For use / installation, the requirements of EN 60079-14 must be ob-

served.

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pH ISM Qualification Kit 11

The digital sensor circuit is part of a common intrinsically safe

system and is for operation connected to a separately certified

transmitter.

The digital sensor circuit as part of an intrinsically safe system is

isolated from the not-intrinsically safe electric circuits up to a maxi-

mum rated voltage of 375 V and from grounded parts up to a

maximum rated voltage of 30 V.

2.7.2 Rated data

Measuring circuit:

Fail-safe ignition protection class Ex ia IIC only for connection to a

certified fail-safe circuit.

Digital pH sensor simulator maximum values:

Two-wire current circuit:

U

i

≤16 V

I

i

≤ 30 mA

P

i

≤ 50 mW

L

i

= negligible

C

i

= negligible

Note: The above maximum values are each the total of all individual

circuits of the associated intrinsically safe power supply and trans-

mitter.

pH ISM Qualification Kit © 12/2018 Mettler-Toledo GmbH, Greifensee

52 300 439 E Printed in Switzerland

12 pH ISM Qualification Kit

2.7.3 Special conditions

– The relationship between the maximum permissible ambient

or media temperature and temperature class, for category 1G

applications, zone 0, is shown in the following table :

Temperature class Max. environment resp.

media temperature

T 6 62 °C

T 5 74 °C

T 4 102 °C

T 3 154 °C

– The capacitance and inductance of the connecting cable has to

be considered.

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pH ISM Qualification Kit 13

2.8 Ex-classification FM approved

2.8.1 Introduction

The following FM control drawing and the standards listed in section

2.8.4 must be observed, where applicable:

a

pappapprapproapprovapproveapprovedapproved

a

pappapprapproapprovapproveapprovedapproved

pH ISM Qualification Kit © 12/2018 Mettler-Toledo GmbH, Greifensee

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14 pH ISM Qualification Kit

2.8.2 Rated data

For rated data please observe section 2.7.2.

2.8.3 Special conditions

In type of protection intrinsically safe apparatus, the analytical probes

(pH ISM sensor simulators) equipment is designated with the

following specific conditions of use.

1. The pH ISM sensor simulators shall be installed in compliance

with the enclosure, mounting, spacing and segregation require-

ments of the ultimate application, including a tool removable

cover.

2. Process temperature no greater than +130 ºC.

3. Potential Electrostatic Charging Hazard – To prevent the risk of

electrostatic sparking, the non-metallic surface should only be

cleaned with a damp cloth.

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pH ISM Qualification Kit 15

2.8.4 Applied Standards

United States Standards

Canadian Standards

Title Number Issue

Date

Approval Standard for Electrical Equip ment for

Use in Hazardous (Classified) Locations –

General Requirements.

FM Class 3600 2011

Approval Standard for Intrinsically Safe

Apparatus and Associated Apparatus for Use

in Class I, II & III, Division 1, Hazardous

(Classified) Locations.

FM Class 3610 2015

Approval Standard for Electrical Equip ment for

Measurement, Control and Laboratory Use.

FM Class 3810 2005

Explosive Atmospheres – Part 0: Equipment –

General Requirements.

ANSI/ISA-60079-0

(12.00.01)

2005

Explosive Atmospheres – Part 11: Equip ment

Protection by Intrinsic Safety ”i”.

ANSI/ISA-60079-11

(12.02.01)

2009

Safety Requirements for Electrical Equip ment

for Measurement, Control, and La bo ratory Use

– Part 1: General Requirements.

ANSI/ISA-61010-1

(82.02.01)

2004

Title Number Issue

Date

Explosive Atmospheres –

Part 0: Equipment – General Requirements.

CAN/CSA-C22.2

No. 60079-0

2005

Explosive Atmospheres – Part 11: Equipment

Protection by Intrinsic Safety ”i”.

CAN/CSA-C22.2

No. 60079-11

2009

Safety Requirements for Electrical Equip-

ment for Measurement, Control, and Labora-

tory Use – Part 1: General Requirements.

CAN/CSA-C22.2

No. 61010-1

2004

pH ISM Qualification Kit © 12/2018 Mettler-Toledo GmbH, Greifensee

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16 pH ISM Qualification Kit

3 Product Description

The pH ISM Qualification Kit is a set of 5 different sensor plug-in

heads and allows the simulation of reading values of pH ISM sensors

with predefined values and errors (not changeable by the user) to

assure safe use as qualification tool.

Each sensor plug-in head corresponds to one of METTLER TOLEDO’s

pH ISM sensors and delivers the complete data of an ISM sensor.

The pH ISM Qualification Kit has basically 2 functions:

– Tool for the qualification of measuring systems.

– Service tool for quick checks and loop trouble-shooting.

The data indicated (primary/secondary) and transmitted are as fol-

low:

– Main measured value

– Temperature

– Error message according to indication.

All standard process and wear data of the sensor are also available

in each plug-in head and are also sent to the transmitter or the PLC

as well as to the iSense software.

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pH ISM Qualification Kit 17

4 Operation

4.1 Connecting the transmitter

to the pH ISM Qualification Kit

To qualify your measuring systems proceed as follows:

Please refer to the transmitter instruction manual for the exact de-

scription of the transmitter operation.

Step 1: Disconnect the ISM sensor from the measuring point.

Step 2: Connect one of the pH ISM Qualification Kit plug-in heads

to the transmitter via the standard connecting cable.

Step 3: The preregistered values then are displayed on the trans-

mitter.

Step 4: Check if the displayed values by the transmitter or the PLC

correspond to the predefined fixed values of the pH ISM

Qualification Kit plug-in head.

See certification for exact values and tolerances.

Step 5: In case you are using the Error simulators, check that the

appropriate errors are correctly displayed by the transmitter

or the PLC.

Step 6: Report results into the attached spreadsheet “Protocol for

pH ISM Qualification Kit”.

Problem solving: If any of the tests described above failed, you

should change the connecting cable and repeat the test. If the test

still shows the same result, the transmitter or the cable is defective.

If you are using a transmitter with current outputs, so ensure the out-

puts are correctly wired.

You must never do a calibration (the simulators are read-only).

You must never increment autoclave cycles (always set “NO” to

cycle counter), this is only needed if autoclave has been set to a val-

ue higher than 0.

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18 pH ISM Qualification Kit

Different transmitters may display different values and errors.

Out of range behavior is also different depending on the transmitter

in use thus different values/readings may occur.

Set the transmitter input filter to off (only for SIM pH TGL).

Do not use the pH ISM plug-in heads after the expiry date

shown the label of each plug-in head. Please send them back to

METTLER TOLEDO for recertification.

Environment operating and storing conditions:

Permissible ambient temperature (operation):

–25°C to 60°C (–13°F to 140°F)

Permissible ambient temperature (storage/transport):

–25°C to 60°C (–13°F to 140°F)

Connecting pH ISM

Qualifying plug-in head

Measuring point with

METTLER TOLEDO Electrode

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pH ISM Qualification Kit 19

5 Product Specification

5.1 Simulator, Pre-registered Values

Order No. Product Legend pH Value Temp.

Designation

SIM pH Kit Order No. 52 300 410

52 300 411 SIM PH4 SIM PH4 pH 4.00 80°C

52 300 412 SIM PH7 SIM PH7 pH 7.00 25°C

52 300 413 SIM PH TGL Toggle Mode 30 sec pH 4.00 80 °C

& pH 7.00 & 25°C

52 300 414 SIM PH ERR1 Glass Breakage pH 7.00 25°C

52 300 415 SIM PH ERR2 Fail Temperature Range pH 10.67 – 28 °C

5.2 Sensor Wear Data

Sensor Wear Monitor pH Transmitters M400/M420 /M700/M800

Time to Maintenance (TTM) 20 d

Life Time Indicator (DLI) 245 d

Adaptive Cal Timer (ACT) 7 d

Sensor operating time 55 d

Autoclaving cycles 1

CIP cycles 7

SIP cycles 3

Max temperature 130 °C dd.mm.yyyy (date of production)

Exceptions

52 300 414 (SIM pH ERR1) TTM = 0 d / DLI = 0 d / ACT = 0 d

52 300 415 (SIM pH ERR2) TTM = 0 d / DLI = 0 d / ACT = 0 d

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20 pH ISM Qualification Kit

5.3 Warnings and Alarms

52 300 414 (SIM pH ERR1) Incident: Glass breakage

Transmitter Warnings/Alarms

M300 Error pH Gls Res < 5MΩ

M400 Error pH Gls Res < 5MΩ

M420 Error pH Gls Res < 5MΩ (Err 15)

M700 Fail Glass impedance

Warn Cal timer

Warn TTM Maintenance timer

M800 Error pH Gls Res < 5MΩ

Maint Required

Cal Required

Change Sensor

52 300 415 (SIM pH ERR2) Incident: Temperature range failure

Transmitter Warnings/Alarms

M300 Error pH Gls change < 0.3

M400 Error pH Gls change < 0.3

M420 Error pH Gls change < 0.3 (Err 13)

M700 Fail Temperature Range

Fail pH Range

Warn Cal timer

Warn TTM Maintenance timer

M800 Warning pH Gls change <0.3

Maint Required

Cal Required

Change Sensor

Please refer to your transmitter instruction manual for specific

instructions.

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