wtw Oxi 330i Mode d'emploi

ba52307edfs04 06/2004

ba52307edfs

Oxi 330i

Oxi 340i

Operating manual

Bedienungsanleitung

Mode d’emploi

Instrucciones de operación

Dissolved Oxygen Pocket Meter

Page 3

Sauerstoff-Taschenmeßgerät

Seite 17

Oxymètres de poche

Page 29

Medidor manual del oxígeno disuelto

Página 41

AR

R

C

L

S

T

O

C

A

L

M

O

6

7

1

9

2

7

O

°

C

m

g/l

ARng

TP

Oxi 330i/340i

2

Note to this

operating manual

This operating manual contains a description of

l all basic functions,

l all instructions for a safe operation, and

l all technical data in a compact form.

A more detailed description with notes for special applications is available as

a pdf document via internet under http://www.WTW.com.

Hinweise zu dieser

Bedienungs-

anleitung

Diese Bedienungsanleitung enthält in kompakter Form

l die Beschreibung aller Grundfunktionen,

l alle Hinweise für den sicheren Betrieb und

l alle technischen Daten.

Eine ausführlichere Beschreibung mit Hinweisen für besondere Anwendun-

gen ist als pdf-Dokument im Internet unter http://www.WTW.com erhältlich.

Remarque à ce

mode d’emploi

Ce mode d'emploi contient sous forme compacte

l la description de toutes les fonctions de base et

l toutes les informations assurant un fonctionnement sûr, ainsi que

l tous les données techniques.

Une description plus étendue contenant les informations sur des emplois

spéciaux peut être obtenue sous forme pdf dans l'internet sous http://

www.WTW.com.

Observación

a estas

instrucciones

Este manual de instrucciones incluye la descripción en forma resumida de

l todas las funciones básicas,

l todas las observaciones que le garantizan el

l funcionamiento normal y seguro, asimismo todo las especificaciones y

datos técnicos.

En el internet, bajo http://www.WTW.com encuentra Ud. una descripción

más detallada, en formato pdf, para aplicaciones especiales.

Copyright

Oxi 330i/340i List of contents

3

Oxi 330i/340i - List of contents

Safety . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4

Display and jack field . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4

Mains power ( Oxi 340i only) . . . . . . . . . . . . . . . . . . . . . . . . . . 5

Switching on the measuring instrument . . . . . . . . . . . . . . . . . . 5

Measuring. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 6

Calibration procedure: . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 7

Saving data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 9

Outputting the data memory. . . . . . . . . . . . . . . . . . . . . . . . . . . 9

Transmitting data (only Oxi 340i) . . . . . . . . . . . . . . . . . . . . . . 9

Configuring. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 10

Resetting to default settings. . . . . . . . . . . . . . . . . . . . . . . . . . 11

Technical data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 12

Safety Oxi 330i/340i

4

Safety

instructions

The individual chapters of this operating manual use the following safety in-

struction to indicate various types of danger:

Warning

indicates instructions that must be followed precisely in order to avoid the

possibility of slight injuries or damage to the instrument or the environment.

Display and jack field

Display

Jack field

Warning

Only connect sensors to the measuring instrument that cannot return any

voltages or currents that are not allowed (> SELV and > current circuit with

current limiting). Almost all sensors - in particular WTW sensors - fulfill these

conditions.

AutoCal DIN

AutoCalTEC

mV/pH

1/

cm

K

/

%

°

F

TDS

UpH Sal

S/

m

cm

M

Lin

Tref25

Tref20

nLF

RCL

Auto

Store

Time

Baud

Day.Month No.

Ident

Year

S

8

8.

8

O

C

%

mg/l

LoBat

ARng

AR

TP

1

Cal

°

mbar

Sal

Status display indicator

Measured value display

Function and

Temperature display

Sensor symbol

1 Oxygen sensor

2 Plug-in power supply ( Oxi 340i only)

3 RS232 interface or analog output/recorder ( Oxi 340i only)

3

12

Oxi 330i/340i Mains power ( Oxi 340i only)

5

Mains power ( Oxi 340i only)

You can either operate the measuring instrument with batteries or with the

plug-in power supply. The plug-in power supply provides the measuring in-

strument with low voltage (7.5 V ... 12 V DC). This saves the batteries.

Warning

The line voltage at the operating site must lie within the input voltage range

of the original plug-in power supply (see T

ECHNICAL DATA).

Warning

Only use original plug-in power supplies (see T

ECHNICAL DATA).

Switching on the measuring instrument

2

1

3

l Plug the jack (1) into the socket (2) of the measuring instrument.

l Connect the original WTW plug-in power supply (3) to an easily accessi-

ble mains socket.

l Press the <> key.

Display test appears briefly on the display.

After this, the measuring instrument automatically switches to the mea-

suring mode. The display shows the relevant measured value.

Measuring Oxi 330i/340i

6

Measuring

Overview of the measuring modes:

Special functions:

AutoRead

(drift control)

The AutoRead function checks the stability of the measurement signal (ex-

cept for the measurement of the ORP voltage). Activate AutoRead with

<AR>. Press <RUN/ENTER> to start the AutoRead measurement. During

the AutoRead measurement, AR flashes on the display until a stable mea-

sured value is reached. This can be terminated at any time taking over the

current measured value with

<RUN/ENTER>.

Temperature

measurement

The measuring instrument automatically measures the temperature of the

sample with the integrated temperature sensor of the conductivity measuring

cell (display TP).

AutoRange

measuring range

selection

There are several measuring ranges available for oxygen measurements.

If a measuring range is exceeded, AutoRange causes the measuring instru-

ment to change automatically to the next measuring range. To switch the au-

tomatic measurement range selection on/off, see C

ONFIGURING. When the

AutoRange function is switched on, ARng appears on the display.

Salinity

correction

A salinity correction is required in the oxygen concentration measurement of

samples with a salt content of more than 1 g/l. To do so, press the <CAL>

key repeatedly until Sal appears on the display. Then, enter the salinity with

<▲> <▼>. Then change to the oxygen concentration measuring mode with

<M>.

Switch on the salinity correction with <▲> (display SAL). To switch it off,

press <▼>.

<M> <M>

<M>

Oxygen

concentration

Oxygen

saturation

Oxygen

partial pres-

sure mbar

mg/l

%

Oxi 330i/340i Calibration procedure:

7

Calibration procedure:

Calibration

procedures

The Oxi 330i/340i provides 2 calibration procedures:

l Calibration in water vapor-saturated air. Use the OxiCal

®

-SL air calibra-

tion vessel (accessories) for the calibration.

l Calibration via a comparison measurement (e. g. Winkler titration accord-

ing to DIN EN 25813 or ISO 5813). At the same time, the relative slope is

adapted to the comparison measurement by a correction factor.

Sensor evaluation After the calibration, the measuring instrument evaluates the current status

of the sensor against the relative slope. The evaluation appears on the dis-

play. The relative slope has no effect on the measuring accuracy. Low values

indicate that the electrolyte will soon be depleted and the probe will have to

be regenerated.

Display Relative slope

S = 0.8 ... 1.25

S = 0.7 ... 0.8

S = 0.6 ... 0.7

E3

Invalid calibration

S < 0.6 or S > 1.25

Calibration procedure: Oxi 330i/340i

8

Procedure for calibrating with the air calibration vessel OxiCal®-SL:

Procedure for calibrating via a comparison measurement:

Note

If the correction factor deviates from 1.000, the display of the measured value

units flashes.

l Keep the OxiCal

®

-SL air calibration vessel ready.

l Connect the D. O. probe to the measuring instrument.

l Put the D. O. probe into the air calibration vessel.

l Press the <CAL> key repeatedly until O

2

CAL appears.

l Press <RUN/ENTER>. The AutoRead measurement begins.

l If the measured value is stable, the instrument displays the value of the

relative slope and the sensor evaluation.

l Switch to the measuring mode with <M>.

6

7

1

A

L

C

O

°

C

TP

Cal

6

7

1

8

0

O

°

C

TP

Cal

AR

S

l Connect the D. O. probe to the measuring instrument.

l Press the <CAL> key repeatedly until O

2

FAC appears.

l Immerse the oxygen sensor in the calibrating solution.

l Press <RUN/ENTER>. The AutoRead measurement begins.

l When the measured value is stable, the instrument displays the deter-

mined measured value and the correction factor of the relative slope (ini-

tial value = 1.000).

l Remove the oxygen sensor from the calibrating solution.

l Perform a comparison measurement (determine the nominal value).

Leave the measuring instrument switched on until the nominal value is

determined.

l Set the displayed value on the measuring instrument to the nominal val-

ue with <▲> <▼>. This changes the related correction factor of the rela-

tive slope.

l Switch to the measuring mode with <M>.

6

7

1

A

C

F

O

°

C

TP

Cal

4

2

4

O

mg/l

1

AR

Cal

7

0

ARng

Oxi 330i/340i Saving data

9

Saving data

manually

Press the <STO> key in the measuring mode (display No. with the number of

the next free memory location). Then, press <RUN/ENTER> and enter the ID

number with <▲> <▼>. Terminate the save with <RUN/ENTER>. The instru-

ment changes to the measuring mode.

Saving data

automatically

Int 1

The portable measuring instrument Oxi 330i/340i has an internal data mem-

ory. It can store up to 800 datasets. The save interval (Int 1) determines the

chronological interval between automatic save processes.

To set up the save interval, press <STO> while pressing the <RUN/ENTER>

key (display Int 1) and set the interval with <▲> <▼> key. Then, press

<RUN/ENTER> and enter the ID number with <▲> <▼>. Change to the last

active measuring mode with <RUN/ENTER>. The automatic save is switched

on (display Auto Store)

Outputting the data memory

You can output the data memory with the <RCL> key. By repeatedly press-

ing the <RCL> key, you reach the following functions:

Start the output with <RUN/ENTER>.

Transmitting data (only Oxi 340i)

Transmitting data

manually

Press the <RUN/ENTER> key in the measuring mode.

This manually triggers a data transmission of the current measured value to

the serial interface at any time - independently of the selected intervals.

Transmitting data

automatically

Int 2

The interval to the data transmission (Int 2) determines the chronological in-

terval between automatic data transmissions. After the selected interval ex-

pires, the current data record is transmitted to the interface. To set up the

transmission interval, press <RCL> while holding down the <RUN/ENTER>

key (display Int 2). Then, set the interval with <▲> <▼>.

StO dISP Output stored data on the display

StO SEr Output stored data via the serial interface (only Oxi 340i)

CAL dISP Output calibration data on the display

CAL SEr Output calibration data via the serial interface (only Oxi 340i)

Configuring Oxi 330i/340i

10

Configuring

Note

You can leave the configuration menu at any time with <M>. The parameters

already changed are stored.

Procedure for configuring (factory settings appear in bold typeface):

l Switch off the measuring instrument.

l While pressing the <M> key, press <>.

l Select the required Baud rate with <▲> <▼>.

Selection: 1200, 2400, 4800, 9600 Baud.

l Then press the <RUN/ENTER> key.

l The air pressure is only displayed if an oxygen sensor is connected. Oth-

erwise, "---" appears.

l Continue with the <RUN/ENTER> key.

l Select the required calibration interval for oxygen measurements with

<▲> <▼>.

Selection: 1... 14... 999 d.

l Then press the <RUN/ENTER> key.

l Switch the automatic measuring range selection AutoRange on/off with

<▲> <▼>.

Selection: YES (On), no (Off).

l Then press the <RUN/ENTER> key.

l Select the date and time step-by-step with <▲> <▼>. In between, press

the <RUN/ENTER> key each time.

l When the last <RUN/ENTER> key has been pressed, the instrument

changes to the last active measuring mode.

Baud

0

40

8

mbar

9

4

9

p

Time

4

d

T

3

n

1

O

S

E

Y

ARng

n

r

A

Day.Month

4

00

9

Oxi 330i/340i Resetting to default settings

11

Resetting to default settings

You can reset the measurement parameters and the configuration to the de-

livery status separately from one another (initialization).

Measurement

parameters

The following measurement parameters can be reset to the delivery status:

Configuration

parameters

The following configuration parameters (InI) can be reset to the delivery sta-

tus:

Procedure of the reset:

Oxygen (O

2

InI)

Measuring mode D. O. concentration

AutoRange automatic switchover of

the measurement range

On (YES)

Relative slope 1.00

Correction factor of the relative

slope

1.000

Salinity input 0.0

Salinity correction off

Baud rate 4800

Interval 1

(automatically saved) OFF

Interval 2

(for data transmission, only

Oxi 340i)

OFF

l To switch it off, press <CAL> while pressing the <RUN/ENTER> key.

l To reset the measurement parameters with <▲> <▼>, select YES and

confirm with <RUN/ENTER>, or

l Continue to the configuration parameters without resetting (InI) with the

<RUN/ENTER> key.

l After the configuration parameters, InI changes the instrument to the last

active measurement mode.

o

n

I

n

I

O

Technical data Oxi 330i/340i

12

Technical data

Dimensions

and weight

Mechanical

structure

Electrical

safety

Test certificates

Ambient

conditions

Oxi measuring

ranges

Length [mm] 172

Width [mm] 80

Height [mm] 37

Weight [kg] approx. 0.3

Type of protection IP 66

Protective class III

cETLus, CE

Storage - 25 °C ... + 65 °C

Operation -10 °C ... + 55 °C

Climatic class 2

mg/l % mbar

Measur-

ing range I

Resolu-

tion

0 ... 19.99

(0 ... 19.9 DurOx)

0.01

(0.1 DurOx)

0 ... 199.9

(0 ... 199 DurOx)

0.1

(1 DurOx)

0 ... 199.9

(0 ... 199 DurOx)

0.1

(1 DurOx)

Measur-

ing range

II

Resolu-

tion

0 ... 90.0

(0 ... 90 DurOx)

0.1

(1 DurOx)

0 ... 600

(0 ... 600 DurOx)

1

(1 DurOx)

0 ... 1250

(0 ... 1250 DurOx)

1

(1 DurOx)

Oxi 330i/340i Technical data

13

Accuracy

(± 1 digit)

Correction

functions

Analog output

(only Cond 340i)

Automatic switchover when the recorder is connected AK 323.

mg/l

Concentration

± 0.5 % of the measured value

at an ambient temperature of 5 °C ... 30 °C

%

Saturation

± 0.5 % of the measured value

when measuring in the range of

± 10 K around the calibration temperature

mbar

Partial pressure

± 0.5 % of the measured value

at an ambient temperature of 5 °C ... 30 °C

Temperature

compensation

< 2 % at 0 ... 40 °C

T [°C] ± 0.1

Salinity correction 0 ... 70.0 SAL

Air pressure correction Automatic through installation of

pressure sensor in the range

500 ... 1100 mbar

Voltage Resolution

Saturation

0 ... 200.0 %

0 ... 600 %

0 ... 2 V

0 ... 600 mV

0.1 %

1 %

Concentration

0...20.00 mg/l

0...100.0 mg/l

0...2 V

0...1 V

0.01 mg/l

0.1 mg/l

Accuracy ± 0.5 % of display value

± 0.1(% saturation)

or

± 0.5 % of the display value ± 0.01 mg/l

Internal resistance < 5 Ohm (current limited to max. 0.2 mA

output current)

Technical data Oxi 330i/340i

14

Serial interface

( Oxi 340i only)

Automatic switchover when a PC or a printer is connected via the cable, AK

340/B or AK 325/S.

Power supply

Guidelines

and norms used

Type RS232, data output

Baud rate Can be set to 1200, 2400, 4800, 9600 Baud

Data bits 8

Stop bit 2

Parity None

Handshake RTS/CTS + Xon/Xoff

Cable length Max. 15 m

Batteries 4 x 1.5 V alkali-manganese batteries, Type AA

Operational life approx. 3000 operating hours

Mains The following applies to all plug-in power supplies:

Connection max. Overvoltage category II

Plug-in power supply unit

(Euro, US , UK, Australian plug)

FRIWO FW7555M/09, 15.1432

Friwo Part. No. 1822089

Input: 100 ... 240 V ~ / 50 ... 60 Hz / 400 mA

Output: 9 V = / 1,5 A

EMC EG guideline 89/336/EWG

EN 61326 A1:1998

EN 61000-3-2 A14:2000

EN 61000-3-3:1995

FCC Class A

Instrument safety EG guideline 73/23/EWG

EN 61010-1 A2:1995

Climatic class VDI/VDE 3540

Type of protection EN 60529:1991

Oxi 330i/340i Technical data

15

FCC Class A Equipment Statement

Note: This equipment has been tested and found to comply with the

limits for a Class A digital device, pursuant to Part 15 of the FCC Rules.

These limits are designed to provide reasonable protection against

harmful interference when the equipment is operated in a commercial

environment. This equipment generates, uses, and can radiate radio

frequency energy and, if not installed and used in accordance with the

instruction manual, may cause harmful interference to radio

communications. Operation of this equipment in a residential area is

likely to cause harmful interference in which case the user will be

required to correct the interference at his own expense.

Technical data Oxi 330i/340i

16

Oxi 340i Inhaltsverzeichnis

17

Oxi 340i - Inhaltsverzeichnis

Sicherheit . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 18

Display und Buchsenfeld . . . . . . . . . . . . . . . . . . . . . . . . . . . . 18

Netzbetrieb (nur Oxi 340i) . . . . . . . . . . . . . . . . . . . . . . . . . . . 19

Meßgerät einschalten. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 19

Messen. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 20

Kalibrieren . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 21

Speichern . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 23

Datenspeicher ausgeben . . . . . . . . . . . . . . . . . . . . . . . . . . . . 23

Daten übertragen (nur Oxi 340i). . . . . . . . . . . . . . . . . . . . . . . 23

Konfigurieren . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 24

Rücksetzen (Reset) auf Grundeinstellungen . . . . . . . . . . . . . 25

Technische Daten . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 26

Sicherheit Oxi 330i/340i

18

Sicherheit

Sicherheits-

hinweise

In den einzelnen Kapiteln dieser Bedienungsanleitung weisen die folgenden

Sicherheitshinweise auf verschiedene Stufen von Gefahren hin:

Achtung

kennzeichnet Hinweise, die genau beachtet werden müssen, um mögliche

leichte Verletzungen oder Schäden am Gerät oder der Umwelt zu vermeiden.

Display und Buchsenfeld

Display

Buchsenfeld

Achtung

Schließen Sie an das Meßgerät nur Sensoren an, die keine unzulässigen

Spannungen oder Ströme (> SELV und > Stromkreis mit Strombegrenzung)

einspeisen können. Nahezu alle Sensoren - insbesondere WTW-Sensoren -

erfüllen diese Bedingungen.

AutoCal DIN

AutoCalTEC

mV/pH

1/

cm

K

/

%

°

F

TDS

UpH Sal

S/

m

cm

M

Lin

Tref25

Tref20

nLF

RCL

Auto

Store

Time

Baud

Day.Month No.

Ident

Year

S

8

8.

8

O

C

%

mg/l

LoBat

ARng

AR

TP

1

Cal

°

mbar

Sal

Statusanzeige

Meßwertanzeige

Funktions- und

Temperaturanzeige

Sensorsymbol

1 Sauerstoffsensor

2 Steckernetzgerät (nur Oxi 340i)

3 RS232 Schnittstelle bzw. Analogausgang/Schreiber (nur Oxi 340i)

3

12

Oxi 330i/340i Netzbetrieb (nur Oxi 340i)

19

Netzbetrieb (nur Oxi 340i)

Sie können das Meßgerät wahlweise mit Batterien oder mit dem Steckernetz-

gerät betreiben. Das Steckernetzgerät versorgt das Meßgerät mit Kleinspan-

nung (7,5 V ... 12 V DC). Die Batterien werden dabei geschont.

Achtung

Die Netzspannung am Einsatzort muß innerhalb des Eingangs-Spannungs-

bereichs des Original-Steckernetzgeräts liegen (siehe T

ECHNISCHE DATEN).

Achtung

Verwenden Sie nur Original-Steckernetzgeräte (siehe T

ECHNISCHE DATEN).

Meßgerät einschalten

2

1

3

l Stecker (1) in die Buchse (2) des Meßgeräts stecken.

l Original WTW-Steckernetzgerät (3) an eine leicht zugängliche Steckdo-

se anschließen

l Taste <> drücken.

Im Display erscheint kurz der Displaytest.

Das Meßgerät schaltet danach automatisch in den Meßmodus. Das Dis-

play zeigt den zugehörigen Meßwert an.

Messen Oxi 330i/340i

20

Messen

Überblick über die Meßmodi:

Spezialfunktionen:

AutoRead

(Driftkontrolle)

Die Funktion AutoRead prüft die Stabilität des Meßsignals (außer bei der

Messung bei Redoxspannung). AutoRead mit <AR> aktivieren. Zum Starten

der AutoRead-Messung <RUN/ENTER> drücken. Während der AutoRead-

Messung blinkt die Anzeige AR, bis ein stabiler Meßwert vorliegt. Ein Ab-

bruch mit Übernahme des aktuellen Meßwerts ist jederzeit mit

<RUN/ENTER> möglich.

Temperatur-

messung

Das Meßgerät mißt die Temperatur der Meßlösung automatisch mit dem in-

tegrierten Temperaturmeßfühler des Sauerstoffsensors (Anzeige TP).

Meßbereichswahl

AutoRange

Für Sauerstoffmessungen stehen mehrere Meßbereiche zur Verfügung.

AutoRange bewirkt, daß das Meßgerät bei Überschreiten eines Meßbereichs

automatisch in den nächsten Meßbereich wechselt. Zum Ein/Ausschalten

der automatischen Meßbereichswahl siehe K

ONFIGURIEREN. Bei eingeschal-

teter Funktion AutoRange erscheint die Anzeige ARng.

Salinitäts-

korrektur

Bei der Sauerstoff-Konzentrationsmessung von Meßlösungen mit einem

Salzgehalt von mehr als 1 g/l ist eine Salinitätskorrektur erforderlich. Dazu

die Taste <CAL> so oft drücken, bis im Display Sal erscheint. Anschließend

mit <▲> <▼> Salinität eingeben. Anschließend mit <M> in den Meßmodus

Sauerstoffkonzentration wechseln.

Salinitätskorrektur mit <▲> einschalten (Anzeige SAL). Zum Ausschalten

<▼> drücken.

<M> <M>

<M>

Sauerstoff-

konzentration

Sauerstoff-

sättigung

Sauerstoff-

partialdruck

mg/l

%mbar

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