Chemglass CG-9506-02 Le manuel du propriétaire

Guardian 5000 Series

Hotplate-Stirrer, e-G51HSRDM

Hotplate-Stirrer, e-G51HS07C

Hotplate, e-G51HP07C

Stirrer, e-G51ST07C

Hotplate-Stirrer, e-G51HS10C

Instruction Manual

EN

ES

FR

DE

IT

PT

SE

NL

DA

FI

NO

PL

CZ

HU

CN

KR

Guardian 5000 Series EN-1

Table of Contents

1 INTRODUCTION ............................................................................................................................................... 2

1.1. Safety Information .................................................................................................................................. 2

1.2. Intended Use .......................................................................................................................................... 2

1.3. Package Contents .................................................................................................................................. 3

1.4. Installation .............................................................................................................................................. 3

1.5. Overview ................................................................................................................................................ 4

1.5.1 Dimensions ......................................................................................................................................... 4

1.5.2 Device Setup ...................................................................................................................................... 9

1.5.3 Display (Hotplate-Stirrers) ................................................................................................................ 13

1.5.4 Display (Hotplate) ............................................................................................................................. 14

1.5.5 Display (Stirrer) .............................................................................................................................. 155

2 OPERATION ................................................................................................................................................. 166

2.1 Getting Ready .................................................................................................................................... 166

2.2 Standby Mode .................................................................................................................................... 166

2.3 Controlling the Stirrer ......................................................................................................................... 177

2.4 Controlling the Top Plate Heater ........................................................................................................ 188

2.5 Using the External Probe ..................................................................................................................... 20

2.6 The Settings Menu ............................................................................................................................... 21

2.6.1 Accessing / Exiting ......................................................................................................................... 221

2.6.2 Features ......................................................................................................................................... 221

2.6.3 Structure & Defaults ......................................................................................................................... 22

2.7 Using the Single Point Calibration Feature ........................................................................................... 23

2.8 Enabling / Disabling the Beeper ........................................................................................................... 27

2.9

 Changing the Power Recovery Setting ................................................................................................. 28

2.10

 Reset to Factory Default Settings ......................................................................................................... 29

3 MAINTENANCE ............................................................................................................................................ 331

3.1 Troubleshooting ................................................................................................................................. 331

3.2 Service Information .............................................................................................................................. 32

4 TECHNICAL DATA ......................................................................................................................................... 32

5 COMPLIANCE ................................................................................................................................................. 33

EN-2 Guardian 5000 Series

1. INTRODUCTION

This manual contains installation, operation and maintenance instructions for the Ohaus Guardian 5000 Series.

Please read the manual completely before using.

1.1. Safety Information

Safety notes are marked with signal words and warning symbols. These show safety issues and warnings. Ignoring

the safety notes may lead to personal injury, damage to the instrument, malfunctions and false results.

WARNING For a hazardous situation with medium risk, possibly resulting in severe injuries or death if not

avoided.

CAUTION For a hazardous situation with low risk, resulting in damage to the device or the property or in loss

of data, or minor or medium injuries if not avoided.

A

TTENTION For important information about the product. May lead to equipment damage if not avoided.

NOTE For useful information about the product.

Warning Symbols

General

hazard

Caution, hot

surface

Electrical shock

hazard

Safety Precautions

WARNING! DO NOT use the Hotplate-Stirrer / Hotplate / Stirrer in explosive atmospheres or with

materials that could cause a hazardous environment from processing. Keep in mind the material flash

point relative to the target temperature that has been set. Also, the user should be aware that the

protection provided by the equipment may be impaired if used with accessories not provided by the

manufacturer.

Always operate unit on a level surface for best performance and maximum safety.

DO NOT lift unit by the top plate.

CAUTION! To avoid electrical shock, completely cut off power to the unit by disconnecting the power

cord from the wall outlet. Disconnect unit from the power supply prior to maintenance and servicing.

Spills should be removed promptly after the unit has cooled down. DO NOT immerse the unit for

cleaning. Alkalis spills, hydrofluoric acid or phosphoric acid spills may damage the unit and lead to

thermal failure.

CAUTION! The top plate can reach 500°C; DO NOT touch the heated surface. Use caution at all times.

Keep the unit away from explosive vapors and clear of papers, drapery, and other flammable materials.

Keep the power cord away from the heater plate.

CAUTION! The rear panel of the 10x10-120V unit runs hot to the touch. Avoid contact during operation.

Allow unit to cool before touching the rear panel.

DO NOT operate the unit at high temperatures without a vessel/sample on the top plate.

DO NOT operate the unit if it shows sign of electrical or mechanical damage.

WARNING! Units are NOT explosion proof. Use caution when heating volatile materials.

Earth Ground – Protective Conductor Terminal. Protective earthing of the equipment is achieved via

connection of the provided power cord to a compatible grounded power outlet.

Alternating Current

1.2. Intended Use

The Ohaus Hotplate-Stirrer / Hotplate / Stirrer are intended for general laboratory use. Safety cannot be

guaranteed if used outside of the intended use.

Guardian 5000 Series EN-3

1.3. Package Contents

• Hotplate-Stirrer / Hotplate / Stirrer Unit

• Power Cord (pre-attached for 10x10-120V units)

• Stir Bars (40 x 8mm and 28.6 x 8mm)

1.4. Installation

Upon receiving the Ohaus Hotplate-Stirrer / Hotplate / Stirrer check to ensure that no damage has occurred during

shipment. It is important that any damage that occurred in transport is detected at the time of unpacking. If you do

find such damage, the carrier must be notified immediately.

After unpacking, place the Hotplate-Stirrer / Hotplate / Stirrer on a level bench or table, away from explosive

vapors. Ensure that the surface on which the unit is placed will withstand typical heat produced by the unit and

place the unit a minimum of six (6) inches from vertical surfaces. Do not position the equipment such that it is

difficult to disconnect the power cord during use. Always place the unit on a sturdy work surface.

The Hotplate-Stirrer / Hotplate / Stirrer is supplied with a 3 conductor, grounded power cord that should be plugged

into a matching standard grounded outlet. If the cord supplied does not meet your needs, please use an approved

power cord that has ratings equal or exceeding those of the originally provided cord and that complies with the

local/national regulations of the country in which the equipment is to be used. Replacement of the plug must be

made by a qualified electrician.

EN-4 Guardian 5000 Series

1.5. Overview

1.5.1 Dimensions

Round Top Hotplate-Stirrer

Note: + 2” diameter center of top plate

++ 800 mL of water in 1 L flask, 38 mm stir bar, 150 rpm and 50°C, 23°C ambient, 8” (20 cm) SS probe

Overall dimensions (L x W x H)

26.7 x 17.3 x 12.7 cm

(10.5 x 6.8 x 5”)

Top plate dimensions: Ø 13.5 cm (5.3”)

Top plate material: Aluminum

Electrical (50/60 Hz):

120 volts ±10%: 8.3 amps

230 volts ±10%: 4.6 amps

Fuses: 10A time-delay, 5x20mm, 250VAC

Temperature range: Ambient +5° to 380°C

Temperature stability of top plate

+

:

± 3% > 100°C, ± 2% ≤ 100°C

Temperature stability with temperature probe

++

:

± 1% > 100°C, ± 1°C ≤ 100°C

Stir capacity: 20 L

Speed range: 60 to 1600 rpm

Speed stability: ± 2%

Weight capacity: Up to 20 kg (44 lbs)

Ship weight: 2.8 kg

Guardian 5000 Series EN-5

7×7 Hotplate-Stirrer

Overall dimensions (L x W x H)

30.7 x 22.4 x 12.2 cm

(

12.1 x 8.8 x 4.8”

)

Top plate dimensions: 17.8 x 17.8 cm (7 x 7”)

Top plate material: Ceramic

Electrical (50/60 Hz):

120 volts ±10%: 10.0 amps

230 volts ±10%: 6.0 amps

Fuses: 10A time-delay, 5x20mm, 250VAC

Temperature range: Ambient +5° to 500°C

Temperature stability of top plate

+

:

± 3% > 100°C, ± 2% ≤ 100°C

Temperature stability with temperature probe

++

:

± 1% > 100°C, ± 1°C ≤ 100°C

Stir capacity: 15 L

Speed range: 60 to 1600 rpm

Speed stability: ± 2%

Weight capacity: Up to 15 kg (33 lbs)

Ship weight: 2.8 kg

Note: + 2” diameter center of top plate

++ 800 mL of water in 1 L flask, 38 mm stir bar, 150 rpm and 50°C, 23°C ambient, 8” (20 cm) SS probe

EN-6 Guardian 5000 Series

7x7 Hotplate

Overall dimensions (L x W x H)

30.7 x 22.4 x 12.2 cm

(12.1 x 8.8 x 4.8”)

Top plate dimensions: 17.8 x 17.8 cm (7 x 7”)

Top plate material: Ceramic

Electrical (50/60 Hz):

120 volts ±10%: 10.0 amps

230 volts ±10%: 6.0 amps

Fuses: 10A time-delay, 5x20mm, 250VAC

Temperature range: Ambient +5° to 500°C

Temperature stability of top plate

+

:

± 3% > 100°C, ± 2% ≤ 100°C

Temperature stability with temperature probe

++

:

± 1% > 100°C, ± 1°C ≤ 100°C

Weight capacity: Up to 15 kg (33 lbs)

Ship wei

g

ht: 2.8 k

g

Note: + 2” diameter center of top plate

++ 800 mL of water in 1 L flask and 50°C, 23°C ambient, 8” (20 cm) SS probe

Guardian 5000 Series EN-7

7x7 Stirrer

Overall dimensions (L x W x H)

30.7 x 22.4 x 12.2 cm

(12.1 x 8.8 x 4.8”)

Top plate dimensions: 17.8 x 17.8 cm (7 x 7”)

Top plate material: Ceramic

Electrical (50/60 Hz):

120 volts ±10%: 1.0 amps

230 volts ±10%: 0.5 amps

Fuses: 5A quick-acting, 5x20mm, 250VAC

Stir capacity:

15 L

Speed range: 60 to 1600 rpm

Speed stability:

± 2%

Weight capacity: Up to 15 kg (33 lbs)

Ship weight: 2.8 kg

EN-8 Guardian 5000 Series

10X10 Hotplate-Stirrer

Overall dimensions (L x W x H)

42.2 x 28.6 x 12.2 cm

(16.6 x 11.25 x 4.8”)

Top plate dimensions: 25.4 x 25.4 cm

(

10 x 10”

)

Top plate material: Ceramic

Electrical (50/60 Hz):

120 volts ±10%: 11.2 amps

230 volts ±10%: 7.0 amps

Fuses:

120 volts: 15A quick-acting, 6.3x32mm, 125VAC

230 volts: 10A time-delay, 5x20mm, 250VAC

Temperature range: Ambient +5° to 500°C

Temperature stability of top plate+: ± 3% > 100°C, ± 2% ≤ 100°C

Temperature stability with temperature probe++: ± 1% > 100°C, ± 1°C ≤ 100°C

Stir capacity: 18 L

Speed range: 60 to 1600 rpm

Speed stability: ± 2%

Weight capacity: Up to 18 kg (39 lbs)

Ship weight: 5.4 kg

Note: + 2” diameter center of top plate

++ 800 mL of water in 1 L flask, 38 mm stir bar, 150 rpm and 50°C, 23°C ambient, 8” (20 cm) SS probe

Guardian 5000 Series EN-9

1.5.2 Device Setup

Hotplate-Stirrer (Round Top, 7x7, 10x10-230V)

A. Display Screen

B. Standby Indicator

C. Left Knob: Controls temperature and settings

menu

D. Right Knob: Controls speed

E. External RTD Probe Port

F. Fuse

G. Power Entry Module (PEM)

H. Threaded Knob for Accessory Rod

I. Standby Switch

J. Feet: Not adjustable

EN-10 Guardian 5000 Series

Hotplate-Stirrer (10x10-120V)

A. Display Screen

B. Standby Indicator

C. Left Knob: Controls temperature and settings menu

D. Right Knob: Controls speed

E. External RTD Probe Port

G. Power Cord

H. Threaded Knob for Accessory Rod

I. Standby Switch

J. Feet: Not adjustable

Guardian 5000 Series EN-11

Hotplate (7x7)

A. Display Screen

B. Standby Indicator

C. Knob: Controls temperature and settings menu

E. External RTD Probe Port

F. Fuse

G. Power Entry Module (PEM)

H. Threaded Knob for Accessory Rod

I. Standby Switch

J. Feet: Not adjustable

EN-12 Guardian 5000 Series

Stirrer (7x7)

A. Display Screen

B. Standby Indicator

D. Knob: Controls speed

F. Fuse

G. Power Entry Module (PEM)

H. Threaded Knob for Accessory Rod

I. Standby Switch

J. Feet: Not adjustable

Guardian 5000 Series EN-13

1.5.3 Display (Hotplate-Stirrers)

L. Heater Temperature: Switches to external probe temperature when the probe is plugged in and P is

illuminated.

M. Heater Indicator: Illuminates when heater is running.

N. Heat Setting Indicator: Switches Heater Temperature (L) to Heat Setting when illuminated.

O. Single Point Calibration Icon

P. External Probe Icon

Q. Hot Top Caution Indicator: Illuminates when the heater is ≥ 40°C.

R. Speed Setting Indicator: Illuminates until stirrer reaches the Speed Setting (S).

S. Speed Setting

T. Stirrer Indicator: Illuminates when stirrer is running

EN-14 Guardian 5000 Series

1.5.4 Display (Hotplate)

L. Heater Temperature: Switches to external probe temperature when the probe is plugged in and P is

illuminated.

M. Heater Indicator: Illuminates when heater is running.

N. Heat Setting Indicator: Switches Heater Temperature (L) to Heat Setting when illuminated.

O. Single Point Calibration Icon

P. External Probe Icon

Q. Hot Top Caution Indicator: Illuminates when the heater is ≥ 40°C.

Guardian 5000 Series EN-15

1.5.5 Display (Stirrer)

R. Speed Setting Indicato

r

: Illuminates until stirrer reaches the Speed Setting (S).

S. Speed Setting

T. Stirrer Indicator: Illuminates when stirrer is running

EN-16 Guardian 5000 Series

2 OPERATION

2.1 Getting Ready

To get ready:

1. Plug the female end of the provided power cord into

PEM (G) on the rear side of the unit.

Note: For the 10x10-120V unit, this end of the power

cord is fixed to the rear side of the unit.

2. Plug the male end of the power cord into a matching

standard grounded outlet.

3. The unit will beep once and the screen will illuminate

with three displays:

a) The first will display the unit type (left) and the

software version (right).

b) The second will display the unit’s electrical

power (left) and frequency (right).

c) The third will be the unit’s main operating

screen.

Note: If the third screen is blank and the red

standby indicator (B) to the left of the screen is

illuminated, the unit is in standby mode.

2.2 Standby Mode

1. The rocker switch (I) on the right side of the unit

controls standby mode.

2. When the unit is switched off:

a) All heating and stirring functions will turn off.

b) The screen will be blank and the standby

indicator (B) to the left of the screen will be

illuminated.

If the heater temperature is above 40°C, the

hot top caution indicator will remain

illuminated as well as the current top plate

temperature and “HOT”.

3. When the unit is switched on:

a) All heating and stirring functions will remain

off.

b) The main operating screen will return.

Previous heating and stirring settings will be

displayed.

c) The unit is ready for normal use.

Guardian 5000 Series EN-17

2.3 Controlling the Stirrer

STIRRING OPERATING TIPS

The stirrer increases speed at a steady rate until the setpoint is reached. If the stirrer is not reaching its setpoint: 1)

the stir bar may be too large, 2) the liquid may be too viscous, 3) the setpoint speed may need to be reduced.

Additionally, the magnetic strength of stir bars reduce over time and may need to be replaced.

When heating and stirring a reaction vessel within an oil bath or similar set-up, the stirring function will stir up to

approximately one inch (2.5 cm) from the top plate. The stirring speed will vary according to liquid viscosity, spin

bar length, and distance from top plate. Adjust one or all of these to achieve the desired stirring speed. For

example: the closer the reaction vessel is to the top plate, the strong the magnetic connection between the unit and

the stir bar.

1. Rotate the right knob (D) to control the speed setting

(S).

a) Clockwise rotation will increase the speed

setting (S).

b) Counterclockwise rotation will decrease the

speed setting (S).

2. To turn on the stirrer, press and hold the right knob

(D) until the unit beeps and the stirrer indicator (T)

illuminates.

a) The unit will beep once to confirm the stirrer

has been turned on.

b) The stirrer indicator (T) next to the “RPM”

symbol will blink to indicate that the stirrer is

on and ramping to the target speed.

c) Once the stirrer has reached the target speed,

the speed setting indicator (R) will disappear

and the stirrer indicator (T) will stop blinking

and remain illuminated.

3. To change the speed setting while the stirrer is on:

a) Rotate the right knob (D) to the new speed

setting.

The speed setting (S) will blink to indicate that

the speed setting is not confirmed.

b) Briefly press the right knob (D) to confirm the

new speed setting.

The speed setting (S) will stop blinking once

the new setting is confirmed.

Note: If the speed setting (S) remains idle without

confirmation for 6 seconds, it will reset to the

current setting.

4. To turn off the stirrer, press and hold the right knob

(D) until the unit beeps and the stirrer indicator (T)

disappears.

a) The unit will beep once to confirm the stirrer

has been turned off.

b) The stirrer indicator (T) next to the “RPM”

symbol will disappear to indicate that the

stirrer is off.

c) The speed setting indicator (R) will illuminate.

EN-18 Guardian 5000 Series

2.4 Controlling the Top Plate Heater

1. Rotate the left knob (C) to control the heat setting (L).

a) Clockwise rotation will increase the heat

setting (L).

b) Counterclockwise rotation will decrease the

heat setting (L).

2. To turn on the heater, press and hold the left knob

(C) until the unit beeps and the heater indicator (M)

illuminates.

a) The unit will beep once to confirm the heater

has been turned on.

b) The heater indicator (M) will illuminate next to

the “°C” symbol to indicate that the heater is

running.

c) The current heater temperature (L) will be

alternately displayed with the heat setting (L)

in the top left region of the screen.

d) When the heater temperature (L) is above

40°C, the hot top caution indicator (Q) will be

illuminated.

3. To change the heat setting (L) while the heater is on:

a) Rotate the left knob (C) to the new heat

setting.

The heat setting (L) will blink to indicate that

the heat setting is not confirmed.

The heat setting indicator (N) will illuminate.

b) Briefly press the left knob (C) to confirm the

new heat setting.

The heat setting (L) will stop blinking once the

new setting is confirmed.

If the heat setting (L) remains idle without

confirmation for 6 seconds, it will reset to the

current setting.

4. To turn off the heater, press and hold the left knob

(C) until the unit beeps and the heater indicator (M)

disappears.

a) The unit will beep once to confirm the heater

has been turned off.

b) The heater indicator (M) next to the “°C”

symbol will disappear to indicate that the

heater is off.

CAUTION: This does not mean that the top

plate is safe to touch.

c) Once the heater temperature (L) cools below

40°C, the hot top caution indicator (Q) will

disappear.

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