Thermo Fisher Scientific Dionex Easion Ion Chromatography System Guide d'installation

Marque: Thermo Fisher Scientific

Modèle: Dionex Easion Ion Chromatography System

Taper: Guide d'installation

Dionex Easion Ion Chromatography

System Installation Instructions

Document No. 155032

Revision 01

August 2020

Chromeleon and OnGuard are registered trademarks of Thermo Fisher Scientific Inc.

in the United States.

Microsoft and Windows are registered trademarks of Microsoft Corporation in the

United States and other countries.

All other trademarks are the property of Thermo Fisher Scientific Inc. and its

subsidiaries.

Thermo Fisher Scientific Inc. provides this document to its customers with a product

purchase to use in the product operation. This document is copyright protected and

any reproduction of the whole or any part of this document is strictly prohibited,

except with the written authorization of Thermo Fisher Scientific Inc.

The contents of this document are subject to change without notice. All technical

information in this document is for reference purposes only. System configurations

and specifications in this document supersede all previous information received by

the purchaser.

Thermo Fisher Scientific Inc. makes no representations that this document is

complete, accurate or error-free and assumes no responsibility and will not be

liable for any errors, omissions, damage or loss that might result from any use of

this document, even if the information in the document is followed properly.

This document is not part of any sales contract between Thermo Fisher Scientific

Inc. and a purchaser. This document shall in no way govern or modify any Terms and

Conditions of Sale, which Terms and Conditions of Sale shall govern all conflicting

information between the two documents.

Revision history: Revision 01 released August 2020; new product support

Software version: Chromeleon 7.2.10 MUa and later

For Research Use Only. Not for use in diagnostic procedures.

Doc. 155032-01 08/2020 i

1 • Introduction. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1

1.1 Related Documentation . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1

1.2 Safety Information . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2

1.2.1 Safety Messages and Notes . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2

1.2.2 Safety Symbols . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4

1.3 Regulatory Compliance . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4

1.3.1 Notice on Lifting and Handling of Thermo Scientific

Instruments . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 5

1.3.2 Notice on the Proper Use of Thermo Scientific Instruments . . . 5

1.3.3 Notice on the Susceptibility to Electromagnetic Transmission . 5

1.3.4 WEEE Compliance . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 5

2 • Unpacking Instructions. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 7

2.1 Unpacking the Dionex Easion . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 7

2.2 Unpacking the PC . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 7

3 • System Setup. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 9

3.1 Facility Requirements . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 9

3.2 Connecting the Autosampler (Optional) . . . . . . . . . . . . . . . . . . . . . . . . . 9

3.3 Connecting to the Chromeleon PC . . . . . . . . . . . . . . . . . . . . . . . . . . . . 10

3.3.1 Connecting the Dionex Easion Directly to the PC . . . . . . . . . . 11

Contents

Dionex Easion Installation Instructions

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3.3.2 Connecting the Dionex Easion to an External Hub . . . . . . . . . .13

3.4 Connecting the Dionex Easion Power Cord . . . . . . . . . . . . . . . . . . . . . .14

3.5 Configuring Device Properties . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .15

3.6 Connecting to the Chromeleon ePanel . . . . . . . . . . . . . . . . . . . . . . . . . .17

4 • System Plumbing . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .19

4.1 Preparing Eluent . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .19

4.2 Preparing Regenerant . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .19

4.3 Connecting Bottle Lines . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .21

4.4 Hydrating the Suppressor . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .21

4.5 Setting Up Waste Lines . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .21

4.6 Setting the Eluent Volume . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .22

4.7 Verifying Communication . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .23

4.8 Priming the Pump . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .23

4.9 Plumbing the System . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .25

4.10 Flushing the System . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .26

4.11 Flushing the Columns . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .26

4.12 Installing the Columns . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .27

4.13 Connecting the Backpressure Coils . . . . . . . . . . . . . . . . . . . . . . . . . . . .28

4.14 Installing the Suppressor . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .28

4.15 Filling the Regenerant Line . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .28

4.16 Equilibrating the System . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .29

4.17 Verifying Operational Status . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .30

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1 • Introduction

This manual provides instructions for the initial installation of the Thermo

Scientific™ Dionex™ Easion™ Ion Chromatography System. The Dionex Easion

is an integrated system consisting of a pump, an injection valve, and a

conductivity cell. Other system components (guard column, separator column,

and suppressor) are ordered separately.

The Dionex Easion is controlled with a PC (personal computer) running

Windows® 10 or Windows® 8.1 operating system and the Thermo Scientific™

Dionex™ Chromeleon™ 7 Chromatography Data System (version 7.2.10 MUa and

later). Chromeleon provides complete instrument control, data acquisition, and

data management.

Follow the installation instructions in the order presented here. These instructions

have been carefully developed to ensure that the system installation is successful.

1.1 Related Documentation

The following documents are available for download from the Thermo Fisher

Scientific website or by contacting your local office.

•Thermo Scientific Dionex Easion Ion Chromatography System Operator’s

Manual (Document No. 155028)

•Thermo Scientific Dionex AS-DV Autosampler Operator’s Manual

(Document No. 065259)

•Manuals for columns and other consumable products, including:

Thermo Scientific Dionex CRS 500 Product Manual (Document No. 031727)

Thermo Scientific Dionex OnGuard II Cartridges Product Manual (Document

No. 031688)

Thermo Scientific Dionex Guardcap Product Manual (Document No.

065705)

•Chromeleon 7 Installation Guide (Document No. 7229.0003)

Dionex Easion Installation Instructions

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1.2 Safety Information

The Dionex Easion is manufactured by Thermo Fisher Scientific (Shanghai)

Instruments Company, Ltd. at the following location:

Jinqiao Export Processing Zone, Pu Dong

T71-6 No. 211, Qin Qiao Road

201206 Shanghai

People’s Republic of China

The Dionex Easion is designed for IC (ion chromatography) applications and

should not be used for any other purpose. Operation of a Dionex Easion in a

manner not specified by Thermo Fisher Scientific may result in personal injury.

If there is a question regarding appropriate usage, contact Technical Support for

Dionex products before proceeding:

•In the U.S. and Canada, call 1-800-532-4752 and select option 2.

•Outside the U.S. and Canada, call the nearest Thermo Fisher Scientific office.

1.2.1 Safety Messages and Notes

This manual contains warnings and precautionary statements that can

prevent personal injury and/or damage to the Dionex Easion when

properly followed. Safety messages appear in bold type and are

accompanied by icons, as shown below.

Indicates an imminently hazardous situation which, if not avoided, will

result in death or serious injury.

Indicates a potentially hazardous situation which, if not avoided,

could result in death or serious injury.

Indicates a potentially hazardous situation which, if not avoided, may

result in minor or moderate injury. Also used to identify a situation or

practice that may seriously damage the instrument, but will not cause

injury.

Indicates that the function or process of the instrument may be

impaired. Operation does not constitute a hazard.

1 • Introduction

Doc. 155032-01 08/2020 3

Messages d'avertissement en français

Warnhinweise in Deutsch

Notes

Informational messages also appear throughout this manual. These are

labeled NOTE and are in bold type:

NOTE NOTES call attention to certain information. They

alert you to an unexpected result of an action,

suggest how to optimize instrument performance,

and so on.

Signale une situation de danger immédiat qui, si elle n'est pas évitée,

entraînera des blessures graves à mortelles.

Signale une situation de danger potentiel qui, si elle n'est pas évitée,

pourrait entraîner des blessures graves à mortelles.

Signale une situation de danger potentiel qui, si elle n'est pas évitée,

pourrait entraîner des blessures mineures à modérées. Également

utilisé pour signaler une situation ou une pratique qui pourrait

gravement endommager l'instrument mais qui n'entraînera pas de

blessures.

Bedeutet unmittelbare Gefahr. Mißachtung kann zum Tod oder

schwerwiegenden Verletzungen führen.

Bedeutet eine mögliche Gefährdung. Mißachtung kann zum Tod oder

schwerwiegenden Verletzungen führen.

Bedeutet eine mögliche Gefährdung. Mißachtung kann zu kleineren

oder mittelschweren Verletzungen führen. Wird auch verwendet, wenn

eine Situation zu schweren Schäden am Gerät führen kann, jedoch

keine Verletzungsgefahr besteht.

Dionex Easion Installation Instructions

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1.2.2 Safety Symbols

These symbols appear on the Dionex Easion or on Dionex Easion labels:

1.3 Regulatory Compliance

Thermo Fisher Scientific performs complete testing and evaluation of its products

to ensure full compliance with applicable domestic and international regulations.

When the Dionex Easion is delivered to you, it meets all pertinent international

electromagnetic compatibility (EMC), safety, and material compliance

requirements and directives.

Changes that you make to your system may void compliance with one or more of

these requirements and directives. Changes to your system include replacing a

part or adding components, options, or peripherals not specifically authorized and

qualified by Thermo Fisher Scientific. To ensure continued compliance with these

requirements and directives, replacement parts and additional components,

options, and peripherals must be ordered from Thermo Fisher Scientific or one of

its authorized representatives.

For additional details, please refer to the CE Declaration of Conformity available

on the Thermo Fisher Scientific website.

Alternating current

Primary protective conductor terminal

Secondary protective conductor terminal

Power supply is on

Power supply is off

Indicates a potential hazard. Refer to this manual for an

explanation of the hazard and how to proceed.

1 • Introduction

Doc. 155032-01 08/2020 5

1.3.1 Notice on Lifting and Handling of Thermo Scientific

Instruments

For your safety, and in compliance with international regulations, the

physical handling of this Thermo Fisher Scientific instrument requires a

team effort to lift and/or move the instrument. This instrument is too

heavy and/or bulky for one person alone to handle safely.

1.3.2 Notice on the Proper Use of Thermo Scientific

Instruments

In compliance with international regulations: This instrument must be

used in the manner specified by Thermo Fisher Scientific to ensure

protections provided by the instrument are not impaired. Deviations from

specified instructions on the proper use of the instrument include changes

to the system and parts replacement. Accordingly, order replacement parts

from Thermo Fisher Scientific or one of its authorized representatives.

1.3.3 Notice on the Susceptibility to Electromagnetic

Transmission

Your instrument is designed to work in a controlled electromagnetic

environment. Do not use radio frequency transmitters, such as mobile

phones, in close proximity to the instrument.

For manufacturing location, see the label on the instrument.

1.3.4 WEEE Compliance

This product is required to comply with the European Union’s Waste

Electrical & Electronic Equipment (WEEE) Directive 2012/19/EU. It is

marked with the following symbol:

This symbol indicates that the equipment must not be thrown into general

waste and should be collected separately and processed in accordance

with local and state requirements.

Dionex Easion Installation Instructions

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Conformité DEEE

Ce produit est conforme avec la directive européenne (2012/19/EU) des

Déchets d'Equipements Electriques et Electroniques (DEEE). Il est

marqué par le symbole suivant:

Ce symbole indique que l'équipement ne doit pas être jeté avec les déchets

ordinaires, mais doit être collecté séparément et traité conformément aux

règlementations locales et nationales.

WEEE Konformität

Dieses Produkt entspricht der EU Waste Electrical & Electronic

Equipment (WEEE) Richtlinie 2012/19/EU. Es ist mit dem folgenden

Symbol gekennzeichnet:

Instrumente mit diesem Zeichen sind nicht für den normallen Abfall

bestimmt; Entsorgung soll den lokalen Vorschriften entsprechend

ausgeführt werden.

Doc. 155032-01 08/2020 7

2 • Unpacking Instructions

This chapter provides instructions for unpacking the Dionex Easion and the PC on

which Chromeleon software is installed.

2.1 Unpacking the Dionex Easion

1. Open the shipping container.

2. Remove the foam and all packed items (bottles, Ship Kit, and so on) from the

top of the container and place them on a workbench.

3. Using the cardboard side handles, carefully lift the Dionex Easion out of the

container and set it on the workbench.

4. Remove the cardboard and foam cradle.

5. Remove the polyethylene bag.

6. Inspect the Dionex Easion for any shipping damage.

7. Save the container and all packing material. You will need them in future if

the system is shipped.

2.2 Unpacking the PC

1. Open the PC box.

2. Remove the PC and all documentation from the box and place them on a

workbench.

3. Follow the instructions in the PC installation guide to connect the PC

components.

Dionex Easion Installation Instructions

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3 • System Setup

This chapter provides instructions for connecting the Dionex Easion to the PC on

which Chromeleon software is installed and configuring IC system properties in

the Chromeleon Instrument Configuration Manager. It also describes autosampler

connections, if required.

3.1 Facility Requirements

Make sure the installation site meets the following environmental specifications.

•Main Power: 90 to 265 Vac, 47 to 63 Hz (auto-sensing power supply; no

manual voltage or frequency adjustment required)

•Operating Temperature: 10 to 35 °C (50 to 95 °F)

•Humidity: 5% to 95% relative humidity, noncondensing

•Provide a sturdy workbench for the Dionex Easion. The workbench height

should ensure convenient access to the interior of the system.

•Allow at least 15 cm (6 in) behind the Dionex Easion for power connections

and ventilation. For optimal performance, install the system in a draft-free

location, out of the path of air conditioning and heating vents.

•Use ASTM Type I (18.2 megohm-cm) filtered and deionized water when

preparing eluent and regenerant.

3.2 Connecting the Autosampler (Optional)

If the system includes a Thermo Scientific™ Dionex™ AS-DV Autosampler, place

the autosampler to the left of the Dionex Easion on the workbench.

Connect the sample out line from the Dionex AS-DV to port S(5) on the injection

valve inside the Dionex Easion (see Figure 3-1). For detailed connection

instructions, refer to the Dionex AS-DV operator’s manual.

Dionex Easion Installation Instructions

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3.3 Connecting to the Chromeleon PC

The Dionex Easion rear panel provides a USB receptacle for connecting to a USB

port on the PC on which Chromeleon is installed. There are two options for

connecting the system to the PC:

•Connect the Dionex Easion directly to a USB port on the PC.

–or–

•Connect the Dionex Easion to an external USB 2.0 hub, and then connect the

hub to the PC.

An external hub(s) is required in the following situations:

•When the number of USB devices in the system exceeds the number of

available USB ports.

–or–

•When the Dionex Easion or other USB device is more than 5 meters (16 ft)

from the PC.

All USB connections described here require standard A-to-B cables (see

Figure 3-2).

Figure 3-1. Dionex Easion Injection Valve

The USB standard limits the USB cable length to 5 meters (16 ft). Each

USB device can be separated from the PC by no more than five hubs.

Thus, each USB device can be located no more than 30 meters

(32 yds) from the PC.

Dionex AS-DV

Sample Out Line

3 • System Setup

Doc. 155032-01 08/2020 11

3.3.1 Connecting the Dionex Easion Directly to the PC

Prerequisites

Check that the following tasks have been completed. If necessary,

complete them now. For instructions, refer to Chromeleon 7 Installation

Guide.

•Chromeleon software was installed.

•The Chromeleon license was installed.

To connect the system to the PC:

1. Locate the USB cable (P/N 960777) provided in the Dionex Easion

Ship Kit (P/N 067768).

2. Plug the “A” connector of the USB cable into a USB port on the

Chromeleon PC (see Figure 3-3).

3. Plug the “B” connector of the USB cable into the USB receptacle on

the Dionex Easion rear panel (see Figure 3-4).

Figure 3-2. USB A-to-B Cable

Before connecting the USB cable, verify that Chromeleon is installed.

If not, Windows will be unable to identify the new USB device when

the power is turned on.

Do not turn on the power to the Dionex Easion (or any other USB

modules) until after you connect the USB cable.

Dionex Easion Installation Instructions

12 Doc. 155032-01 08/2020

Figure 3-3. Example USB Connections: IC System Connected to the PC

Figure 3-4. Dionex Easion Rear Panel

USB Cable

System

USB

Receptacle

Power

Receptacle

3 • System Setup

Doc. 155032-01 08/2020 13

3.3.2 Connecting the Dionex Easion to an External Hub

The Dionex Easion Ship Kit (P/N 067768) includes one USB cable

(P/N 960777). A configuration with an external hub requires at least one

additional USB cable.

Prerequisites

Check that the following tasks have been completed. If necessary,

complete them now. For instructions, refer to Chromeleon 7 Installation

Guide.

•Chromeleon software was installed.

•The Chromeleon license was installed.

To connect the system to an external hub:

Refer to Figure 3-5 to connect the Dionex Easion, the PC, and any

additional devices (for example, a Dionex AS-DV) to an external USB

hub. Refer to the manual provided by the hub vendor for complete

installation instructions.

Before connecting the USB cable, verify that Chromeleon is installed.

If not, Windows will be unable to identify the new USB device when

the power is turned on.

Do not turn on the power to the Dionex Easion (or any other USB

modules) until after you connect the USB cable.

Dionex Easion Installation Instructions

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3.4 Connecting the Dionex Easion Power Cord

1. Verify that the main power switch on the rear panel of the Dionex Easion (see

Figure 3-4) is turned off. (The main power switch may have been turned on

accidentally when the system was unpacked.)

2. Connect the power cord (IEC 320 C13) (ordered separately) from the main

power receptacle on the Dionex Easion rear panel to a grounded power

source. The Dionex Easion power supply is auto-sensing; this means that no

adjustment is required to select the line voltage.

Figure 3-5. Example USB Connections: Multiple Devices Connected to an

External Hub

The USB standard limits the USB cable length to 5 meters (16 ft). Each

USB device can be separated from the PC by no more than five hubs.

Thus, each USB device can be located no more than 30 meters

(32 yds) from the PC.

SHOCK HAZARD—To avoid electrical shock, use a grounded

receptacle. Do not operate the Dionex Easion or connect it to AC

power mains without an earthed ground connection.

The power supply cord is used as the main disconnect device. Make

sure the socket-outlet is located near the Dionex Easion and is easily

accessible.

3 • System Setup

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3.5 Configuring Device Properties

When the Dionex Easion (or other device) is added to an instrument in

Chromeleon, default configuration properties are assigned automatically. If the

default settings are not correct for your system, you can change them.

Prerequisites

Check that the following tasks have been completed. If necessary, complete them

now. For instructions, refer to Chromeleon 7 Installation Guide.

•The USB device driver was installed.

•An instrument was created in the Chromeleon Instrument Configuration

Manager.

•The Dionex Easion was assigned to the Chromeleon instrument.

To start the Instrument Configuration Manager: On the Windows taskbar, click

Start > All Programs > Thermo Chromeleon 7 > Instrument Configuration

Manager.

Operation at AC input levels outside of the specified operating voltage

range may damage the Dionex Easion.

DANGER D'ÉLECTROCUTION—Pour éviter toute électrocution, il faut

utiliser une prise de courant avec prise de terre. Ne l'utilisez pas et ne

le branchez pas au secteur C.A. sans utiliser de branchement mis à la

terre.

Le cordon d'alimentation principal est utilisé comme dispositif

principal de débranchement. Veillez à ce que la prise de base soit

située/installée près du module et facilement accessible.

STROMSCHLAGGEFAHR—Zur Vermeidung von elektrischen

Schlägen ist eine geerdete Steckdose zu verwenden. Das Gerät darf

nicht ohne Erdung betrieben bzw. an Wechselstrom angeschlossen

werden.

Das Netzkabel ist das wichtigste Mittel zur Stromunterbrechung.

Stellen Sie sicher, daß sich die Steckdose nahe am Gerät befindet und

leicht zugänglich ist.

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To configure the Dionex Easion:

1. In the Instrument Configuration Manager, verify that the correct device is

assigned to control the Dionex Easion injection valve.

a. In the Properties dialog box for the Dionex Easion, click the Inject Valve

tab.

b. For Pump_InjectValve, verify the Controlled By setting.

If the instrument includes a Dionex AS-DV, the Controlled By setting

must be AS.

If the instrument does not include a Dionex AS-DV, the Controlled By

setting must be Dionex Easion.

To change a Controlled By setting: Select the Pump_InjectValve name,

press F2, and select the correct device.

2. Check the detection limits, standby flow rate, and inactivity time-out period

settings.

a. In the Properties dialog box, click the Options tab.

b. Under Set Detection Limits, verify that the default conductivity range (0

to 500 S) is selected. The larger range (0 to 10,000 S) is used only for

specialized applications.

c. To have the pump flow rate automatically reduced after a period of

inactivity, select a Standby Flow Rate and an Inactivity Time Out

Period. To disable this feature, set the time out period to 0 (Off).

3. Select the TTL and relay output settings.

a. In the Properties dialog box, click the State Devices tab.

b. Select the check boxes for the TTL and relay outputs you plan to use.

Clear the check boxes for the outputs you do not plan to use.

c. If a Dionex AS-DV is installed, verify that Pump_ECD_Relay_1 is

selected.

4. Click OK to close the Properties dialog box.

5. Click File > Save Installation.

6. If the “no inject device installed” message appears, ignore it and click Close.

(This message appears when the instrument does not include an autosampler

because you are doing manual injections.)

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Thermo Fisher Scientific Dionex Easion Ion Chromatography System Guide d'installation

Marque: Thermo Fisher Scientific

Modèle: Dionex Easion Ion Chromatography System

Taper: Guide d'installation

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