Ohaus ST5000-B Manuel utilisateur

STARTER 5000

Bench pH Meter

Instruction Manual

STARTER 5000

Medidor de pH de banco

Manual de instrucciones

STARTER 5000

PH-mètre de laboratoire

Manuel d’instructions

TABLE OF CONTENTS

1 INTRODUCTION ................................................................ 1

1.1 Definition of Signal Warnings and Symbols ................................. 1

1.2 Safety Precautions ........................................................................... 2

2 INSTALLATION ................................................................. 3

2.1 Package contents ............................................................................. 3

2.2 Installing the stand-alone electrode holder ................................... 4

2.3 Installing the power adapter ........................................................... 4

2.4 Connect the pH electrodes ............................................................. 5

3 DISPLAY AND ICONS ....................................................... 5

3.1 Turn on the meter ............................................................................. 5

3.2 Turn off the meter............................................................................. 6

3.3 Icons .................................................................................................. 6

3.4 Menu directory ................................................................................. 9

4 CALIBRATION, MEASUREMENT AND PRINT .............. 10

4.1 Calibration ...................................................................................... 10

4.1.1 Buffer group ..................................................................................... 10

4.1.2 Performing calibration ....................................................................... 11

4.2 Sample measurement .................................................................... 12

4.2.1 pH measurement ............................................................................. 12

4.2.2 mV and Rel.mV measurement ......................................................... 12

4.3 Temperature measurement ........................................................... 12

4.4 Printing ............................................................................................ 13

5 SETUP ............................................................................. 14

5.1 System Setting ............................................................................... 14

5.1.1 System setting ►Save Mode .......................................................... 14

5.1.2 System Setting ►Output ................................................................. 14

5.1.3 System Setting ► Restore Factory Setup ....................................... 14

5.1.4 System Setting ► Service Password .............................................. 14

5.2 Measurement Setting ..................................................................... 15

5.2.1 Measurement Setting ►Endpoint Mode .......................................... 15

5.2.2 Measurement Setting ►GLP Measurement Mode .......................... 15

5.2.3 Measurement Setting ►Continuous Measure ................................. 15

5.3 Calibration Setting ......................................................................... 16

5.3.1 Calibration Setting ►Buffer Group .................................................. 16

5.3.2 Calibration Setting ►Calibration Reminder ..................................... 16

5.4 Data Log .......................................................................................... 16

6 MAINTENANCE ............................................................... 17

6.1 Error message ................................................................................ 17

6.2 Meter maintenance ........................................................................ 17

6.3 Electrode maintenance .................................................................. 17

6.4 Information ..................................................................................... 17

7 TECHNICAL DATA .......................................................... 18

7.1 Specifications ................................................................................. 18

8 COMPLIANCE ................................................................. 19

9 BUFFER GROUPS .......................................................... 20

STARTER 5000 Bench pH Meter EN-1

1 INTRODUCTION

Thank you for choosing this OHAUS product.

Please read the manual completely before using the STARTER 5000 bench pH meter to avoid

incorrect operation.

STARTER 5000 is a 0.001pH bench meter with a color touch-screen LCD. It’s a new generation of

intuitive and easy-to-use bench meters for reliable measurements.

A few of the many existing features are:

 Bi-lingual graphical user interface

 Auto, manual time endpoint which can assist users to freeze the stable reading value to

meet different customer requirements

 8 buffer groups (US, EU, NIST and JJG) with 1 self-defined buffer

 IP54 water and dust protection

1.1 Definition of Signal Warnings and Symbols

Safety notes are marked with signal words and warning symbols. These show safety issues and

warnings. Ignoring the safety notes may lead to personal injury, damage to the instrument,

malfunctions and false results.

Signal Words

WARNING For a hazardous situation with medium risk, possibly resulting in

injuries or death if not avoided.

CAUTION For a hazardous situation with low risk, resulting in damage to the

device or the property or in loss of data, or injuries if not avoided.

Attention For important information about the product

Note For useful information about the product

Warning Symbols

General Hazard Electrical Shock Hazard

Explosion Hazard Corrosive Hazard

Alternating Current Direct Current

EN-2 STARTER 5000 Bench pH Meter

1.2 Safety Precautions

CAUTION Read all safety warnings before installing, making connections, or

servicing this equipment. Failure to comply with these warnings could result in

personal injury and/or property damage. Retain all instructions for future reference.

 Verify that the AC adapter's input voltage range and the plug type are compatible with the

local AC power supply.

 Make sure that the power cord does not pose a potential obstacle or tripping hazard.

 Use the equipment only in dry locations.

 Dry off any liquid spills immediately. The instrument is not watertight.

 Use only approved accessories and peripherals.

 Operate the equipment only under ambient conditions specified in these instructions.

 Disconnect the equipment from the power supply when cleaning.

 Do not operate the equipment in hazardous or unstable environments.

 Service should only be performed by authorized personnel.

 If the equipment is used in a manner not specified by the manufacturer, the protection

provided by the equipment may be impaired.

WARNING Do not use this instrument in an environment subject to explosion

hazards. The housing of the instrument is not gas tight (explosion hazard due to

spark formation, corrosion caused by the ingress of gases).

CAUTION When using chemicals and solvents, comply with the instructions of the

producer and the general lab safety rules.

STARTER 5000 Bench pH Meter EN-3

2 INSTALLATION

Carefully unpack the box.

2.1 Package contents

The model ST5000-B (basic package) has the following items:

In addition to ST5000-B content, the ST5000-F package also includes the following:

Each pH buffer powder should be dissolved in 250ml pure water or deionized water in a

volumetric flask. You also can order the bottled buffer solution from Ohaus.

More electrodes, solutions, accessories and spare parts, please contact Ohaus for more details.

Model

Description

P/N

ST350

3-in-1 glass refillable pH Electrode

30129354

ST310

3-in-1 plastic refillable pH Electrode

83033965

ST210

2-in-1 plastic refillable pH Electrode

83033966

ST320

3-in-1 plastic gel pH Electrode(no need to fill)

83033967

ST260

2-in 1 glass double salt bridge pH Electrode

30129357

ST230

2-in-1 glass muddy sample pH Electrode

83033968

STSURF

2-in-1 flat surface pH Electrode

30129470

STMICRO5

2-in-1 glass micro sample pH Electrode

30087566

STMICRO8

2-in-1 glass micro sample pH Electrode

30087569

STTEMP30

Temperature Electrode

83033970

STORP1

Gel plastic ORP electrode

30038555

STORP2

Refillable glass ORP electrode

30038553

ST5000-B

Units

ST5000 meter

1

ST5000 In use cover

1

Stand-alone electrode holder

1 set

4GB USB flash drive

1

Buffer powder set (4.01; 7.00; 10.00)

1 set

Power supply

1 set

ST350 3-in-1 glass refillable pH electrode

1

Buffer powder set (4.01; 7.00; 10.0)

83033971

Buffer pH1.68 250ml

30100424

Buffer pH4.01 250ml

30100425

Buffer pH7.00 250ml

30100427

Buffer pH10.01 250ml

30100429

Buffer pH12.45 250ml

30100440

pH electrode Reference Electrolyte

30059255

pH electrode protection solution

30059256

Electrode holder stand alone

30058733

ST5000 In use cover

30129897

SP Cable Adapter RS232 F-M SF40A (for ST5000)

30059316

EN-4 STARTER 5000 Bench pH Meter

2.2 Installing the stand-alone electrode holder

Install the electrode arm on the base:

After adjusting the tension knob to some extent, the upper arm can be move up and down.

When the pH electrode is placed on the arm and calibration or measurement is being

performed, the storage bottle of pH electrode can be placed into the base hole for easy

storage:

2.3 Installing the power adapter

Insert the adapter plug into the power adapter slot.

CAUTION Only use an adapter plug that is compatible with the mains power

receptacle. Make sure that the adapter plug is fully seated in the power adapter slot

before plugging it into the mains power receptacle.

STARTER 5000 Bench pH Meter EN-5

2.4 Connect the pH electrodes

There are 2 sockets for the electrode. “pH” socket (BNC); “TEMP.” Socket (Cinch).

For ST350 3-in-1 electrode, connect both the BNC and Cinch socket. For 2-in-1 pH electrodes

(e.g. ST230), only connect the BNC.

3 DISPLAY AND ICONS

3.1 Turn on the meter

STARTER 5000 is a color touch screen 0.001pH bench meter. It does not have any buttons.

After connecting with power, the meter will turn on, if meter in screen protection, you can tap the

screen to turn on the screen.

Note: If customer did not operate the meter for more than 6 hours, the meter will completely shut

off automatically. You cannot turn on the meter by tapping the screen any more. You need to

reconnect power to turn on the meter.

Select the language and then press to enter the main interface.

Main Interface

EN-6 STARTER 5000 Bench pH Meter

3.2 Turn off the meter

To turn off the meter, please tap the turn-off button in the top-left of main interface to enter

the turn-off interface. Then tap to turn-off the meter or tap to go back to

main interface again.

Turn-off interface

3.3 Icons

User ID

Sample ID

Information icon

Date

Time

pH measurement mode. Shift between mV and Rel.mV mode or

Signal icon, when it is blinking that means the meter is receiving signal (in

measurement or calibration).

Endpoint icons, auto-endpoint, manual-endpoint and time-endpoint.

When in manual-endpoint, if the signal is stable, the meter will show the stable signal

icon. Tap the stop icon to reach manual endpoint.

Signal stable icon

Temperature icon.

STARTER 5000 Bench pH Meter EN-7

Information, measure and calibrate tap area

The information area is also the shortcut to enter the setting interface:

"Endpoint:"

Tap this area to enter the interface to set the endpoint mode. Available

modes are Auto, Manual and Time endpoint. The current endpoint mode is

displayed.

"Sensor ID:"

Tap this area to enter the interface to select, set or change the sensor ID.

The current sensor ID is displayed.

"Sensor Cond:"

Tap this area to enter the sensor calibration data interface. The current

sensor performance icon (judged by calibration data) is displayed.

There are 3 sensor condition icons:

Slope: more than 95%

and offset: ± (0-15) mV

Electrode condition is good

Slope: 90-95%

or offset: ± (15-35) mV

Electrode condition is

acceptable

Slope: less than 90%

or offset: ± (35-60) mV

Electrode condition is not

good or needs cleaning

Calibration reminder icon. Set the time you want the meter to alert you to do

calibration from last calibration. When the time is reached, this icon will be displayed

and blink to remind that it is time to perform a calibration.

“Buffers:”

This area displays the current buffer group, tap this area to enter the interface to

select the buffer group.

Start icon. Tap this icon and the meter will begin measurement, the signal

icon will blink. The start icon area will show the stop icon

Calibration icon. Tap this icon to start calibration.

Save icon. After saving the current measurement result (endpoint reached), this

icon color will change from black to light gray , indicating that the reading has

already been saved and cannot be saved twice.

Output icon. Output data to external device such as a printer.

If “Shut off connection” is chosen in System Setting ►Output, the save

icon will be displayed .Otherwise the output icon will be displayed in the

same position.

EN-8 STARTER 5000 Bench pH Meter

Return to main interface

Return to previous menu

Enter, confirm or apply current setup, finish setting

Edit

Page up

Page down

Delete

Increase (light)

Decrease (light)

Graph display (for the measurement or calibration data)

Save

Output to external device (USB flash drive, printer)

Full keyboard

Next calibration point

Current Calibration point again

End of calibration

STARTER 5000 Bench pH Meter EN-9

3.4 Menu directory

The menus of first and secondary directory for STARTER 5000:

System

Setting

Date

Time

Save Mode

Output

Screen Brightness

Baud Rate

Screen Protection

Restore Factory Setup

Instrument Information

Service Password

Measurement

Setting

Resolution

MTC Temp. Input

pH/mV/Rel.mV Mode

Continuous Measure

Endpoint Mode

ID setting

GLP Measurement Mode

Calibration

Setting

Buffer Group

Calibration Reminder

Data

Measurement Data

Calibration Data

EN-10 STARTER 5000 Bench pH Meter

4 CALIBRATION, MEASUREMENT AND PRINT

The meter display will turn off automatically according to the time set in the menu System Setting

►Screen Protection ►LCD Auto-off. To turn on the screen again, tap the screen.(See 3.1)

A complete pH measurement process should follow the procedure:

a) Rinse the pH electrode and connect to meter

b) Prepare the buffer and calibrate the pH electrode

c) Prepare the sample

d) Conduct pH measurement of the sample

e) Record measurement data

f) Rinse the pH electrode and store

Prepare the pH electrode: the pH electrode should be rinsed with pure water before and after

usage. Check if the electrode is physically damaged. (Be careful with the glass bulb)

The pH electrode should be stored in the storage bottle. After the pH electrode has been put into

the sample or buffer solution, stir several seconds then wait 30 to 60 seconds for the signal to be

stable, and then press the button to operate (Calibration or measurement).

WARNING Do not operate the equipment in hazardous environments. The equipment

is not explosion protected.

CAUTION When using chemicals and solvents, comply with the instructions of the

chemical producer and the general lab safety rules.

4.1 Calibration

4.1.1 Buffer group

STARTER 5000 can perform 1-5 point calibrations for predefined buffer groups. For self-defined

buffer group, it can do 1-9 point calibration.

Before calibration, make sure the current buffer group is the group wanted.

When using a new pH electrode, a calibration should be performed before any measurement. If a

pH electrode is not used for a few days, a calibration should be performed before next usage.

Calibration is to display the right pH value when the meter receive the mV value signal from the

pH electrode.

Slope: the linear coefficient between mV and pH according to theoretical value (e.g. -

59.16mV/pH @ 25°C means 100% slope);

Offset: the mV value when the pH value is 7.00. (Theoretical value is 0 mV)

STARTER 5000 Bench pH Meter EN-11

STARTER 5000 will give an electrode condition icon to show the performance of the pH electrode

according to the calibration data. Normally, if we get sad face icon after a proper calibration, you

may need to replace the pH electrode with a new one.

STARTER 5000 automatically corrects for the temperature dependence of the buffer pH values.

E.g. for US standard buffer group "1.68, 4.01, 7.00, 10.01" reference the following table:

For example, with calibration buffer 10.01 at 15°C , the calibration result should be 10.12 pH.

4.1.2 Performing calibration

After rinsing the pH electrode, put the electrode into the first buffer, stir for 10s then press to

start the calibration. When in calibration, the signal icon blinks. When the endpoint has been

reached, appears while disappears and current point calibration is finished, There

are now 3 options:

Quit the calibration and go back to main interface

Finish current point calibration, go to calibration result interface

Do the next point calibration

Note: During calibrating process, the ST5000 is always in Auto Endpoint Mode.

Note: The use of 3-in-1 pH electrode which include the temperature sensor or a separate

temperature electrode is recommended. When using the MTC mode, enter the correct

temperature value and keep all buffer and sample solutions at the set temperature.

5°C

1.67

4.01

7.09

10.25

10°C

1.67

4.00

7.06

10.18

15°C

1.67

4.00

7.04

10.12

20°C

1.68

4.00

7.02

10.06

25°C

1.68

4.01

7.00

10.01

30°C

1.68

4.01

6.99

9.97

35°C

1.69

4.02

6.98

9.93

40°C

1.69

4.03

6.97

9.89

45°C

1.70

4.05

6.97

9.86

50°C

1.71

4.06

6.96

9.83

EN-12 STARTER 5000 Bench pH Meter

4.2 Sample measurement

4.2.1 pH measurement

Be sure the electrode has been calibrated before measurement. After rinsing,

 Place the pH electrode in the sample.

 Press to start the pH measurement, when the endpoint has been reached, the current

measurement is finished.

Note: If the signal is not stable all the time, it is recommended to use manual endpoint mode to

avoid bad repeatability.

4.2.2 mV and Rel.mV measurement

Press to shift to or mode; follow the same procedure as for pH

measurement to perform mV or Rel.mV measurement.

If the meter is connected to an ORP electrode, the mV result is the value of Oxidation-Reduction

Potential value; also called Redox value.

4.3 Temperature measurement

For better accuracy, we recommend to use either a built-in or a separate temperature electrode.

 If a temperature electrode is used, ATC and the sample temperature are displayed.

 If the meter does not detect a temperature electrode, it automatically switches to the manual

temperature compensation mode and MTC appears. MTC temperature should be set.

Note: STARTER 5000 accepts NTC 30 kΩ temperature sensor. For ATC (Auto Temperature

Compensation) or MTC (Manual Temperature Compensation), the Temperature Compensation

only corrects for the change in the output of the electrode, not for the change in the actual solution.

That means the meter corrects the signal (mV) from the pH electrodes to get a more accurate pH

value according to the real temperature.

STARTER 5000 Bench pH Meter EN-13

4.4 Printing

STARTER 5000 can print the measurement or calibration data through RS232. After the printer

(e.g. OHAUS SF-40A) is connected to the meter properly, make the following settings(See 5.1):

please order the connect cable for ST5000 (P/N 30059316) to connect SF40A and ST5000.

System Setting ► Output , select Printer

System Setting ► Baud Rate, select 9600.

The format for the print-out measurement is:

Date Time User SampleID

6-13-2015 14:20:22 User01 Sample02

SensorID Endpoint mode MTC/ATC

Sensor02 Manual ATC

Temperature Result

25.3°C 6.999pH

The format for the print-out calibration data is:

Calibration Data

SensorID Serial Number

Sensor02 14060012

Cal. Date Cal. Time ATC/MTC

01-01-2015 14:20:33 ATC

Buffers mV Offset Slope

4.00pH 176.94mV

7.00pH 0.05mV 0.05mV 98.22%

When performing continuous measurement, the format for the print-out calibration data is:

Timing Measure Record

SensorID Serial Number

Sensor03 14060012

Date Time Temperature Measurement

01-01-2015 14:20:25 23.5°C 6.998pH

Date Time Temperature Measurement

01-01-2015 14:20:30 23.5°C 6.999pH

Date Time Temperature Measurement

01-01-2015 14:20:35 23.5°C 7.000pH

EN-14 STARTER 5000 Bench pH Meter

5 SETUP

5.1 System Setting

System setting is used to set meter parameters, the meter information could also be found in it.

Please see section 3.4 for reference.

5.1.1 System setting ►Save Mode

Save mode has 2 options, one is Auto Save Endpoint Reading, another is Manual Save Endpoint

Reading. Auto Save Endpoint Reading means that when the measurement reaches the endpoint

(auto, manual or time endpoint), the meter will save the endpoint reading automatically.

The Save icon will change from black to light grey ; An endpoint reading can be

saved only once.

5.1.2 System Setting ►Output

When selecting shut off connection, the main interface will display the save icon , or

display the Output Icon .

5.1.3 System Setting ► Restore Factory Setup

Restoring the factory setup includes the following:

1. Shut off GLP mode

2. Shut off Auto Save mode

3. Shut off continuous measure

4. Shut off (output) connection

5. Shut off calibration Reminder

6. The resolution is: 0.001pH, 0.01mV

7. Measurement mode: pH

8. Self buffer group will be deleted

9. Baud rate: 9600

10. Brightness of screen: 70%

11. Shut off Screen Protection

12. MTC: 25°C

13. Endpoint: Auto

14. Time endpoint: 10 Second

15. Delete all the calibration data

5.1.4 System Setting ► Service Password

Not used.

STARTER 5000 Bench pH Meter EN-15

5.2 Measurement Setting

5.2.1 Measurement Setting ►Endpoint Mode

Auto Endpoint

In this mode, the meter will reach the endpoint and lock the reading according to the following

stability criteria automatically:

0.1pH resolution: the signal of the sensor input may not change by more than 0.3mV in 6

seconds.

0.01pH resolution: the signal of the sensor input may not change by more than 0.1mV in 6

seconds.

0.001pH resolution: the signal of the sensor input may not change by more than 0.03mV in 6

seconds.

Time Endpoint

In this mode, the user needs to input the endpoint time, e.g. 15 seconds. This means after starting

the measurement for 15s, the meter will reach the endpoint.

Manual Endpoint

In this mode, the user needs to decide when the signal reading is stable, then press the stop icon

to reach manual endpoint.

5.2.2 Measurement Setting ►GLP Measurement Mode

GLP mode requires each measurement to have the User ID and Sample ID. If there is no sample

ID or user ID, the meter will show the interface to let user input the required data.

5.2.3 Measurement Setting ►Continuous Measure

During continuous measure, the user needs to input the time interval to get each reading result.

Below is the Graph of continuous measure.

The Y axis is pH value. The x axis is the Number of measurement result.

EN-16 STARTER 5000 Bench pH Meter

5.3 Calibration Setting

5.3.1 Calibration Setting ►Buffer Group

Before calibration, please make sure the current buffer group is correct for your buffer solutions.

User can select from the 8 predefined buffer groups.

User can also set self-defined buffer groups. The adjacent 2 calibration point difference should be

larger than 0.99pH.

5.3.2 Calibration Setting ►Calibration Reminder

Enter this setting to set the time, from the last calibration, after how many hours the meter should

remind to perform calibration again. The meter will show the calibration reminder icon and

blink, to remind user to perform calibration.

5.4 Data Log

Tap Data to get into the Data log interface, including measurement data and calibration data.

You can delete all the measurement data here. The only way to delete calibration data is to

restore factory setup.

The data can be output to a USB Flash Drive (≤4GB).

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