Struers Movipol-3 Manuel utilisateur

Manual No.: 13927003

Date of Release 

Movipol-3

Instruction Manual

Movipol-3

Instruction Manual

Table of Contents Page

User’s Guide .............................................................. 1

Reference Guide ...................................................... 16

Quick Reference Guide ............................................ 21

Always state Serial No and Voltage/frequency if you have technical questions or when ordering spare parts.

You will find the Serial No. and Voltage on the type plate of the machine itself. We may also need the Date

and Article No of the manual. This information is found on the front cover.

The following restrictions should be observed, as violation of the restrictions may cause cancellation of Struers

legal obligations:

Instruction Manuals: Struers Instruction Manual may only be used in connection with Struers equipment

covered by the Instruction Manual.

Service Manuals: Struers Service Manual may only be used by a trained technician authorised by Struers.

The Service Manual may only be used in connection with Struers equipment covered by the Service Manual.

Struers assumes no responsibility for errors in the manual text/illustrations. The information in this manual is

subject to changes without notice. The manual may mention accessories or parts not included in the present

version of the equipment.

The contents of this manual is the property of Struers. Reproduction of any part of this manual without the

written permission of Struers is not allowed.

Struers A/S

Pederstrupvej 84

DK-2750 Ballerup

Denmark

Telephone +45 44 600 800

Fax +45 44 600 801

Movipol-3

Instruction Manual

Movipol-3

Safety Precaution Sheet

To be read carefully

before use

1. The operator must be fully instructed in the use of the apparatus,

according to the User's Guide.

2. The operator must be fully instructed in the use of the electrolytes used

with Movipol-3.

3. Observe the current safety precautions regarding the handling, mixing,

filling and disposal of the electrolyte (see section Safety Precautions).

The Material Safety Data Sheet for each of the Struers electrolytes can

be supplied upon request.

4. Be sure that the actual voltage corresponds to the voltage stated on the

type plate of the apparatus.

5. Check that the apparatus is standing firmly on the support. If the

apparatus is carried or hung by the shoulder strap, check that the strap

is intact and that the buckle is correctly fastened.

6. Always check that the pump motor is working before taking the pencil

out of its holder.

7. Always place the pencil in its holder when it is not used.

8. Do not leave the apparatus unattended when filled with electrolyte.

9. Make sure that the apparatus is safely secured during transportation

and that is does not contain electrolyte.

10. The maximum polishing voltage allowed at the work site must be

observed.

The equipment should only be used for its intended purpose and as detailed in the Instruction Manual.

The equipment is designed for use with consumables supplied by Struers. If subjected to misuse, improper

installation, alteration, neglect, accident or improper repair, Struers will accept no responsibility for damage(s)

to the user or the equipment.

Dismantling of any part of the equipment, during service or repair, should always be performed by a qualified

technician (electromechanical, electronic, mechanical, pneumatic, etc.).

Movipol-3

Instruction Manual

Disposal

Equipment marked with a WEEE symbol contain electrical and

electronic components and must not be disposed of as general

waste.

Please contact your local authorities for information on the correct

method of disposal in accordance with national legislation.

Movipol-3

Instruction Manual

1

User’s Guide

Table of Contents Page

1. Getting Started

Checking the Contents of Packing .................................................... 3

Placing Movipol-3 .............................................................................. 3

Getting Acquainted with Movipol-3 .................................................... 4

Supplying Power ............................................................................... 5

Connecting the Transformer .................................................... 5

Charging the Batteries ...................................................................... 5

Connecting the Pump Motor and Cathode ........................................ 5

Connecting the Anode ....................................................................... 5

External Etching Operations .............................................................. 5

2. Operation

Using the Controls............................................................................. 6

Front Panel Controls ................................................................ 6

Safety Functions ............................................................................... 7

Cut-out of Pump Motor ............................................................. 7

Current Limiter Function of the Polish/Etch Circuit ................... 7

Cut-out of Polish/Etch Circuit ................................................... 7

Cut-out in case of under-voltage .............................................. 7

Mounting the Container ..................................................................... 7

Dismounting the Container ................................................................ 7

Mounting the Pump-Container Unit ................................................... 8

Dismounting the Pump-Container Unit .............................................. 8

Filling Electrolyte into the Container .................................................. 8

Emptying the Container of Electrolyte ............................................... 8

Mounting the Polishing Chamber ...................................................... 8

Starting the Polishing/Etching Process .............................................. 9

Stopping the Polishing/Etching Process ............................................ 9

Cleaning the Container and the Pump ............................................ 11

Voltage Examples ........................................................................... 11

Cast Iron. 3.4% C, 0.29% Si, 0.6% Mn, 0.3% P ..................... 11

Duplex Steel ........................................................................... 11

Commercial Pure Aluminium 99.5% Al ................................... 11

Stainless Steel ....................................................................... 12

Low Carbon Steel 0.1% C ...................................................... 12

High Carbon Steel .................................................................. 12

Titanium Alloys ....................................................................... 12

Movipol-3

Instruction Manual

2

3. Safety precautions

Electricity ......................................................................................... 13

Electrolytes in General .................................................................... 13

Perchloric Acid in Particular ............................................................ 13

Training of Operators ...................................................................... 14

Mixing the Solution .......................................................................... 14

Storage of Perchloric Acid or Solution ............................................. 14

Fire and Explosion Hazards ............................................................ 14

Disposal .......................................................................................... 15

Working with Movipol-3 in the field .................................................. 15

Dangerous Localities .............................................................. 15

Safety Measures .................................................................... 15

Dangerous situations ............................................................. 15

Movipol-3

Instruction Manual

3

1. Getting Started

In the packing box you should find the following parts:

1 Movipol-3 with control unit, pump, pencil

1 Transformer

1 Container for electrolyte

1 Anode wire

1 Anode clamp

1 Magnet

1 Shoulder strap

10 Polishing Chambers

1 Funnel

1 Set of Instruction Manuals

Movipol-3 is a portable apparatus for field electropolishing. If

possible the apparatus should be placed on a stable support. If not it

can be hung by the shoulder trap in a suitable place.

During transportation the apparatus must not contain electrolyte and

should be secured in order not to turn upside down.

Checking the Contents of

Packing

Placing Movipol-3

Movipol-3

Instruction Manual

4

Take a moment to familiarise yourself with the location and names of

the Movipol-3 components.

 Charge/pump switch  Charge indicator

 Start button  Voltage indicator for pump motor

 Adjusting knob for polishing

voltage  Polishing indicator

 Etching indicator

 Adjusting knob for etching

voltage  Socket pump/cathode

 Socket anode

 Polishing time  Socket for external etching

 Etching time 

Pencil

 Ammeter

Getting Acquainted with

Movipol-3

Instruction Manual

5

 Connect the mains cable to the mains.

 Connect the 42V multi plug to the left side of Movipol-3.

 Switch O/Charge - l/Pump to top position, the batteries of

Movipol-3 are now being charged. When the batteries are fully

charged, the Charge Indicator lights green. If the batteries need

charging the Charge Indicator will light red.

Even though the batteries are factory charged, Struers recommends

the charging of Movipol-3 batteries 1-2 hours before operating the

apparatus.

 Connect the multi plug to the socket in the control unit with the

screw cap. Both the electrolyte pump motor and the cathode in

the pencil are now connected to the control unit.

 Place the banana plug of the anode wire in the socket, Anode.

The connection to the sample is established with the enclosed

magnet or clamp.

 When external etching operations should be carried out, i.e.

when using a cathode connection other than the built-in cathode

in the pencil, the black socket, Output Volt 2-90V DC should be

used as cathode connection.

Supplying Power

IMPORTANT

Check that the mains voltage corresponds to the voltage stated on the type

plate on the side of the machine.

Connecting the Transformer

Charging the Batteries

WARNING

A fully charged set of batteries will self-discharge in 6 months, and a

complete discharging may reduce the lifetime. Therefore the batteries

should be charged at regular intervals.

IMPORTANT

When the transformer is being used Movipol-3 should only be operated

when the Charge Indicator lights green or yellow.

Connecting the Pump Motor

and Cathode

Connecting the Anode

External Etching Operations

Movipol-3

Instruction Manual

6

2. Operation

Name Function



O/CHARGE

I/PUMP SWITCH



When switched to O/Charge the

batteries are being charged if

the apparatus is connected to

mains. When switched to l/Pump

the pump motor starts operating.



AMMETER



For reading the amperage

during the polishing/etching

process. The range of 0-2 is

used for polishing. The range of

0-0.2 A is used for etching.

Changing between the ranges is

done automatically when the

timers switch from polishing to

etching.



START BUTTON





Push button for starting the

polishing/etching process.



CHARGE INDICATOR



Indicates the battery charging

level. When connected to 42V

AC possible readings are as

follows:

Battery Charging

Level O/ I/

Charge Pump

Medium charged Yellow Green

Fully charged Green Green

Not Charged Red Red



ADJUSTING KNOB FOR

POLISHING VOLTAGE



Adjusting knob for setting the

voltage for polishing. It can be

set in the range of 10-90 V. The

voltage range of 60-90 volt DC is

marked with a voltage danger

warning.



VOLTAGE INDICATOR

FOR PUMP MOTOR



Indicates whether the pump is

supplied with sufficient voltage:

0: The apparatus is switched off.

Yellow: Pump motor in operation

at sufficient voltage.

Red: Pump motor blocked due

to overload of pump motor or too

low voltage. Electrical circuit

switched off due to overload.



ADJUSTING KNOB FOR

ETCHING VOLTAGE

Adjusting knob for setting the

voltage for etching.



POLISHING

INDICATOR

The Polishing Indicator lights red

when the polishing process is

running and is switched off when

the process is finished.



POLISHING TIME

Adjusting knob for setting the

time of polishing. When set to ∞

the process continues until the

knob is set to zero.



ETCHING INDICATOR

The Etching Indicator lights red

when the etching process is

running and is switched off when

the process is finished.



ETCHING TIME

Adjusting knob for setting the

time of etching. When set to ∞

the process continues until the

knob is set to zero.



SOCKET PUMP/

CATHODE

For connecting the pump motor

and cathode to the control unit.

Using the Controls

Front Panel Controls

Movipol-3

Instruction Manual

7

Name Function



SOCKET

ANODE

For connecting the anode wire to

the control unit.



SOCKET

FOR

EXTERNAL

ETCHING

For connecting the cathode

when external etching

operations should be carried

out.

In case of higher load than 1 A the cut-out function is activated. The

Voltage Indicator for Pump Motor will light red. The apparatus can be

restarted when the error has been eliminated.

In case of a voltage range of 70-90 V the current is limited

corresponding to the maximum effect of the transistors (140 VA).

In case of a voltage range of 2-70 V at 2 A the cut-out function is

activated and an alarming signal is heard. When the error has been

corrected the apparatus can be restarted. In case of overload the

circuit is cut out and the Voltage indicator for Pump Motor lights red.

The apparatus can be restarted after cooling when the indicator

lights yellow.

Under-voltage may occur using insufficiently charged batteries. The

cut out function for under-voltage will disconnect the process and an

alarm signal is heard.

 Place the pump in the container.

 Press down the black knobs and turn them until the markings

turn towards the pump.

 Check that the container is firmly locked.

 Press the two black knobs down and turn them so that the

markings turn away from the pump, a click is heard and the

pump is released from the container.

Safety Functions

Cut-out of Pump Motor

Current Limiter Function of the

Polish/Etch Circuit

Cut-out of Polish/Etch Circuit

Cut-out in case of under-voltage

Mounting the Container

Dismounting the Container

Movipol-3

Instruction Manual

8

 Lower the pump-container unit into the cabinet.

 Press the unit down until a click is heard. The pump-container

unit is now locked in the cabinet.

 Press the two black locks to the sides from the pump in direction

of the cabinet wall, a click is heard and the pump-container unit

is dismounted and can be removed from the cabinet.

 Before filling electrolyte into the container, the section, Safety

Precautions should be carefully observed.

 Remove the pump and container from the cabinet.

 Remove the pump from the electrolyte container.

 Pour the electrolyte into the electrolyte container. The level must

be between the minimum (350 ml) and maximum (750 ml)

marks.

 Mount the container on the pump and mount the unit in the

cabinet of Movipol-3.

 Before emptying the container of electrolyte, the section, Safety

Precautions should be carefully observed.

 Remove the pump-container unit from the cabinet and remove

the container.

 If the electrolyte is to be used again pour the electrolyte carefully

back into the electrolyte bottle. Use the funnel supplied with the

apparatus.

 If the electrolyte is not to be used again it should be filled into a

container suitable for disposal. Please observe the local

regulations and instructions for disposal.

 Press the polishing chamber onto the pencil until it fits tightly.

A polishing chamber has a limited lifetime as the plastic hardens

because of contact with the electrolyte. The chamber should be

renewed regularly.

Mounting the Pump-Container

Unit

Dismounting the Pump-

Container Unit

Filling Electrolyte into the

Container

Emptying the Container of

Electrolyte

IMPORTANT

Funnel, gloves, ventilation as well as all other prescribed equipment must be

used during filling/emptying.

Mounting the Polishing

Chamber

Movipol-3

Instruction Manual

9

 Make sure that the correct type and amount of electrolyte has

been filled in the electrolyte container.

 Connect the anode to the sample by means of the clamp or

magnet supplied with the apparatus.

 Set the polishing voltage and polishing time.

 Set the etching voltage and etching time.

 Activate the pump motor by switching O/Charge - l/Pump to

bottom position.

 Take the pencil from the pencil holder and place it on the spot

which is to be prepared.

 Press the pencil against the surface ensuring that the polishing

chamber is in total contact with the surface.

 Keep the pencil perpendicular (at a angle of 90°) to the surface.

The electrolyte will now begin to circulate.

 Press the button START . A "sensor circuit" records whether

there is electric connection from the cathode in the pencil

through the electrolyte to the anode.

 If the electric circuit is closed the timer starts the process.

 Read the ammeter to check if the correct amperage has been

obtained.

 When both the Polishing and Etching Indicators are switched off

the process has been completed and the pencil should be

placed in the pencil holder.

 When the pencil has been placed in the holder, switch off the

pump motor by switching the O/charge - l/Pump to O/Charge.

 Clean the polished spot with water/alcohol and dry carefully.

 The polishing/etching process can be stopped at any time during

operation by setting the adjusting knob for polishing/etching time

to zero.

Starting the Polishing/Etching

Process

IMPORTANT

Take care that no air is drawn around the periphery of the polishing

chamber.

IMPORTANT

Only press the start button when the noise from the pump indicates that the

flow through the pencil is constant.

Stopping the Polishing/Etching

Process

Movipol-3

Instruction Manual

10

After polishing with one electrolyte or after mechanical polishing, the

sample can be etched using a different electrolyte and the external

etching connection. (External etching accessory required)

 Connect the anode to the sample using the clamp or magnet

supplied with Movipol-3.

 Connect the tongs for external etching to the black socket on the

Movipol-3.

 Set the etching voltage and etching time.

 Pick up a ball of cotton wool with the tongs.

 Dip the cotton wool ball in a suitable electrolyte (e.g. 10% oxalic

acid for stainless steel).

 Start the pump and then the polishing/etching process.

 Swab the specimen surface with the cotton wool, and observe

the movement on the Ammeter.

 Clean the polished spot with water/alcohol and dry carefully.

External Etching

Movipol-3

Instruction Manual

11

The electrolyte container and the pump system must be cleaned with

water after use.

 Empty the container of electrolyte.

 Fill the container with water and start the pump by switching

O/Charge - l/Pump to bottom position to circulate water from the

electrolyte container through the pump system.

Due to graphite inclusions, electrolytic polishing is not ideal, but it is

satisfactory for "testing on the spot". The metallic structure develops

excellently and only the graphite appearance will be less successful.

Due to the softness of the graphite this may be helped by rubbing

the polished surface with a piece of wet cotton wool, perhaps with

AP-Alumina Suspension FF.

Pregrinding with Transpol Up to grit 400

Electrolyte AC-2

Polishing voltage 40V

Polishing current 0.5A

Polishing time 15 sec

Pregrinding with Transpol Up to grit 400

Electrolyte A-2

Polishing

Voltage 35V

Current 0.7A

Time 15 sec

Etching

Voltage 8V

Current 0.2A

Time 12 sec

Pregrinding with Transpol Up to grit 400

Electrolyte A-2

Polishing voltage 85V

Polishing current 0.3A

Polishing time 20 sec

Cleaning the Container and the

Pump

Voltage Examples

Cast Iron. 3.4% C, 0.29%

Si, 0.6% Mn, 0.3% P

Duplex Steel

Commercial Pure Aluminium

99.5% Al

Movipol-3

Instruction Manual

12

Pregrinding with Transpol Up to grit 400

Electrolyte E-5

Polishing voltage 80V

Polishing current 0.6A

Polishing time 10 sec

External etch in 10% Oxalic acid or 10% (NH)2S2O3

Pregrinding with Transpol Up to grit 400

Electrolyte A-2

Polishing

Voltage 60V

Current 0.8A

Time 10 sec

Etching

Voltage 5V

Current 0.18A

Time 5 sec

Pregrinding with Transpol Up to grit 220

Electrolyte A-2

Polishing

Voltage 60V

Current 1.0A

Time 15 sec

Etching

Voltage 3-6V

Current 0.013A

Time 3 sec

Pregrinding with Transpol Up to grit 220

Electrolyte A-3

Polishing voltage 50V

Polishing current 1.0A

Polishing time 15 sec

Stainless Steel

Low Carbon Steel 0.1% C

High Carbon Steel

Titanium Alloys

Movipol-3

Instruction Manual

13

3. Safety precautions

In some working areas a maximum safety voltage is specified. Such

a maximum range would typically be 42V AC (60 DC). Movipol-3 is

used with a 42V AC transformer through a 54V DC re-chargeable

battery set. Movipol-3 can be used according to these restrictions.

Alternatively Movipol-3 may work on batteries only.

When using electrolytes all necessary safety measures should be

taken. Apart from the safety precautions listed in the following, a

material Safety Data Sheet for each of the electrolytes delivered by

Struers can be supplied upon request.

 It is essential that the user(s) is/are fully instructed in the work

procedure of these electrolytes.

 Movipol-3 is designed for use with electrolytes recommended by

Struers. Other electrolytes, e.g. electrolytes containing strong

bases or acids, may harm the construction or endanger the

safety of the user.

NOTE that many electrolytes contain alcohol or other

inflammable solvents. Make sure that all safety

precautions are followed when using such electrolytes.

 When cleaning the apparatus after use, make sure that no

electrolyte is allowed to dry and/or crystallise inside the

apparatus or on the polished material.

 It is essential that the user is fully trained in the use of Movipol-3

and electrolytes involved.

Electrolytes from Struers with the prefix A consist of approx. 1 l stock

solution to which 15 to 90 ml perchloric acid (60%) should be added.

Before mixing the perchloric acid to the stock solution it is of great

importance that the following safety precautions are carefully

observed. Furthermore a Material Safety Data Sheet for the

perchloric acid in question can be supplied upon request.

Electricity

WARNING

The polishing circuit may generate voltages up to 90V DC. The Adjusting

knob for Polishing Volt indicates the critical range from 60 to 90V in yellow.

Electrolytes in General

Perchloric Acid in Particular

Movipol-3

Instruction Manual

14

 All personnel involved in the mixing, use, storage, transportation,

and disposal of the electrolytes or its components, should be

thoroughly trained in the precautions for handling perchloric acid.

 Great importance must be attached to precautions against

inhalation of vapours of the solution or its components, against

skin contact, mixing and overheating, and concerning storage

and disposal methods.

 Place the solvent/water mixture in a water bath with temperature

control. Carefully add the perchloric acid to the solvent/water

mixture, stir continuously.

 The mixing must take place in a ventilated chemical fume hood

designed for perchloric acid use.

 The operator(s) must use the listed protective clothing or

devices: full face shield or splash goggles, rubber gloves and lab

coat or coveralls.

 Avoid the use of any combustible or carbonaceous containers,

reaction vessels, spill pans, storage shelves, or materials of this

type when dealing with the acid.

 Do not permit any acid to crystallise on bottle necks, caps, or

anywhere else.

 Store in secure, cool, and ventilated area with metal, glass, or

ceramic spill catch pan.

 Store away from other chemicals, combustible and organic

materials.

 Do not, under any circumstances, permit solutions to dry out.

 60% perchloric acid is a strongly corrosive and oxidising product.

Heating may cause an explosion and contact with combustible

material may cause fire.

 Fire fighting should be done from a protected location.

Extinguish with water spray only. Do not use dry chemicals or

carbon dioxide.

 Do not produce anhydrous perchloric acid, either from its salts or

from aqueous solutions, e.g. by heating with high boiling acids or

dehydrating agents, such as sulphuric acid or phosphorous

pentoxide. In addition to spontaneous explosion, the anhydrous

acid explodes instantaneously on contact with oxidizable organic

materials.

 The use or storage of perchloric acid should be limited to

quantities less than 500 g per hood.

Training of Operators

Mixing the Solution

Storage of Perchloric Acid or

Solution

Fire and Explosion Hazards

Movipol-3

Instruction Manual

15

Follow local regulations for disposal of spillage and waste.

Dilution and/or neutralisation are the normally recommended

methods of disposal of the electrolyte.

Certain safety measures must be taken when working with Movipol-3

in the field as some working locations can be dangerous. This is the

case when working in:

 Closed containers, e.g. boilers, tanks and fractionating columns.

 Narrow areas such as shafts, pits, pipes and tunnels.

Working in these above mentioned locations can be dangerous as

poisonous substances can be accumulated and as there can be too

little oxygen in the air.

Consequently it is recommended that tanks or other narrow areas

are not opened or entered without written permission.

Necessary preparations and safety precautions should be mentioned

in the permission and it must be issued by the manager in charge of

safety for the actual process line or plant.

No working process should begin without this permission. The safety

precautions and work processes stated for the place of work should

be followed. In case of doubt regarding the contents of the

authorisation, the issuer should be consulted.

Dangerous situations can occur when working in locations with

choking or poisonous gases. In order to make sure that the air can

be breathed without risk it must be analysed. Electric insulation

defects may also involve a safety risk.

However, safe working procedure may be carried out if adequate

safety precautions are taken before and during the work process.

Disposal

Working with Movipol-3

in the field

Dangerous Localities

Safety Measures

Dangerous situations

Movipol-3

Instruction Manual

16

Reference Guide

Table of Contents Page

1. Consumables and Accessories

Accessories for Movipol-3 ............................................................... 17

Supplementary Equipment .............................................................. 17

2. Trouble-shooting

Electrolyte ....................................................................................... 18

Flow ................................................................................................ 18

Pencil and Cathode ......................................................................... 18

Polishing Chamber .......................................................................... 18

Power Supply .................................................................................. 18

3. Maintenance

Pump and Electrolyte Container ...................................................... 19

Every day ............................................................................... 19

Cabinet ........................................................................................... 19

Every day ............................................................................... 19

Every week ............................................................................ 19

Once a year ........................................................................... 19

Exchange of Batteries ..................................................................... 19

4. Technical Data ..................................................................... 20

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