Gilson Minipuls 3 Manuel utilisateur

3

User’s Guide

Peristaltic Pump

User’s Guide

TABLE OF CONTENTS

MINIPULS® 3 PerIStaLtIc PUMP | USer'S GUIde

Table of Contents

Safety | 1

Symbols and Notices | 1

Intended Use | 2

Safety Cover | 3

Operating Conditions | 4

Solvents | 4

Replacement Parts | 4

Sécurité | 5

Symboles et avertissements | 5

Utilisation prévue | 6

Capot de protection | 7

Conditions de fonctionnement | 8

Solvants | 8

Pièces détachées | 8

taBLeOFcONteNtS| MINIPULS® 3 PerIStaLtIc PUMP

TABLE OF CONTENTS

CHAPTER 1 | Introduction | 9

Unpacking | 10

Customer Service | 10

Description | 11

Speed Control Module | 12

Front Panel | 12

Rear Panel | 14

Pump Head with Safety Cover | 15

CHAPTER 2 | Setup | 19

Electrical | 20

Remote Control Connections | 20

Install or Change the Pump Head | 23

Remove Cover | 23

Open Pump Head | 24

Install Pump Head | 25

Tubing - Selection and Fitting | 26

Introduction | 26

Type of Material | 27

Diameter and Flow Rate | 28

Fitting the Tubing | 29

Safety Cover Installation | 33

MINIPULS® 3 PerIStaLtIc PUMP | USer'S GUIde

TABLE OF CONTENTS

Flow Rate Selection and Adjustment | 33

Selection | 33

Adjustment | 33

Recommendations | 37

Gilson Connectors and Couplers | 38

Connectors | 38

Coupling Kits | 40

Couplers | 40

CHAPTER 3 | Operation | 41

Keypad Functions | 42

Initialization | 44

Autostart Function | 46

Non-autostart Mode | 46

Autostart Mode | 46

Hold Mode | 46

Mode Selection | 47

Changing the Unit ID | 48

Routine Maintenance | 48

Troubleshooting | 49

Repair and Return Policies | 50

Before Calling Us | 50

Warranty Repair | 50

Non-Warranty Repair | 50

Return Procedure | 51

Unit End-of-Life | 51

taBLeOFcONteNtS| MINIPULS® 3 PerIStaLtIc PUMP

TABLE OF CONTENTS

CHAPTER 4 | Remote Control | 53

Electrical Contact Control | 54

Start/Stop Input (ContactInput) | 54

Direction Control (Contact Input) | 54

Pump Speed (Analog Input) | 55

Control by Gilson Devices | 55

GSIOC Control | 55

GSIOC Commands | 56

Control Modes | 56

Command Descriptions | 57

Examples | 62

Example 1 | 62

Example 2 | 62

APPENDIX | 63

Part Numbers | 63

Standard Accessory Package | 64

Additional Accessories | 65

Connectors | 65

Polyvinylchloride (PVC) Tubing | 66

Fluoroelastomer Tubing (Iso-Versinic®/Viton®) | 68

Silicone Tubing | 69

Polypropylene (PharMed®) Tubing | 70

Electrical Connector | 71

Technical Speciﬁcations | 72

Chapter 3 | SaFetY

Read this section before installing and operating the pump.

Symbols and Notices

The following internationally recognized electronic and hazard

symbols may appear on the instrument:

Symbol Explanation

Direct current

Protective conductor terminal

| Electrical power ON

O Electrical power OFF

Caution

Mechanical hazard

1

MINIPULS® 3 PERISTALTIC PUMP | USER'S GUIDE

The following safety notices may appear in this document:

WARNING

WARNING indicates a potentially hazardous situation

which, if not avoided, may result in serious injury

CAUTION

CAUTION indicates a potentially hazardous situation

which, if not avoided, may result in minor or moderate

injury

NOTICE

NOTICE indicates a potentially hazardous situation

which, if not avoided, may result in equipment damage

Intended Use

The pump is intended to be used in the laboratory, or similar indoor

environment, by trained technical personnel.

The instrument must not be directly connected to

humans for any purpose.

For safe and proper use of this instrument, it is required that both

operating and service personnel follow the instructions contained in

this guide when installing, cleaning, and maintaining the instrument.

The following safety precautions must be observed during all phases

of operation, service, and repair of the instrument. Failure to comply

with these precautions or with specific warnings elsewhere in this

user’s guide violates safety standards of design, manufacture, and

intended use of the instrument. Gilson assumes no liability for the

customer’s failure to comply with these requirements.

2

INTENDED USE | MINIPULS® 3 PERISTALTIC PUMP

INTENDED USE

The MINIPULS 3 has been certified to safety standards required in

Canada, Europe, and the United States. Refer to the instrument rear

panel label and the Declaration of Conformity document for the

current standards to which the instrument has been found compliant.

Safety Cover

A safety cover is installed on each pump

head.

The safety cover protects the user from

the mechanical hazard present when the

pump head is rotating.

Do not operate the pump without the

safety cover installed.

Figure 1

R2 Pump Head

with Installed

Safety Cover

3

MINIPULS® 3 PERISTALTIC PUMP | USER'S GUIDE

SAFETY COVER

Operating Conditions

Access to the rear panel is necessary because the instrument must be

detached from all voltage sources before service, repair, or exchange

of parts. Allow a minimum of 2.54 cm (1in.) space behind the

instrument for proper fan operation.

Operate the instrument using the approved power supply provided

and only at the voltage specified on the rear panel label of the

instrument.

Solvents

Observe safe laboratory practices when handling solvents. If

dangerous liquids are used, adequate protection such as proper

ventilation, safety glasses, etc., should be used. Refer to the Material

Safety Data Sheets for the solvents before use.

Replacement Parts

Be sure to use only replacement parts specified in this user’s guide.

Do not repair or change parts which are not listed in this user’s guide.

If it is necessary to change parts not listed, please contact your local

Gilson representative.

4

SOLVENTS | MINIPULS® 3 PERISTALTIC PUMP

SOLVENTS

Chapter 4 | SÉCUrItÉ

Merci de lire ces instructions avant toute installation ou utilisation de

MINIPULS 3.

Symboles et avertissements

Les symboles suivants sont susceptibles d’apparaître sur l’instrument:

Symbole Signiﬁcation

Courant continu

Borne de terre de protection

| Sous tension

O Hors tension

Attention

Danger méchanique

5

MINIPULS® 3 PERISTALTIC PUMP | USER'S GUIDE

Les consignes de sécurité suivantes peuvent apparaître dans ce

document:

AVERTISSEMENT

AVERTISSEMENT signale une situation potentiellement

dangereuse qui, si elle n’est pas évitée, peut entraîner

desblessures graves

AT TENTION

ATTENTION signale une situation potentiellement

dangereuse qui, si elle n’est pas évitée, peut entraîner

desblessures mineures ou légères

AVIS

AVIS signale une situation potentiellement

dangereuse qui, si elle n’est pas évitée, peut entraîner

desdommagesmatériels

Utilisation prévue

Cet instrument est destiné à être utilisé dans un environnement de

laboratoire, par un personnel technique qualifié.

AT TENTION

L’instrument ne doit en aucun cas être relié directement

au corps humain.

Pour une utilisation correcte et en toute sécurité, il est nécessaire

que le personnel qui utilise et réalise la maintenance de l’instrument,

suive les instructions contenues dans ce guide lors de l’installation, le

nettoyage et la maintenance de l’instrument.

Les consignes de sécurité suivantes doivent être respectées

durant toutes les phases de fonctionnement, d’entretien ou de

réparation de l’instrument. Le non-respect de ces précautions ou des

avertissements spécifiques mentionnés dans ce guide compromet

les normes de sécurité de conception, de fabrication et d’utilisation

prévue de l’instrument. Gilson décline toute responsabilité en cas

d’’incapacité du client à se conformer à ces exigences.

6

UTILISATION PRÉVUE | MINIPULS® 3 PERISTALTIC PUMP

UTILISATION PRÉVUE

MINIPULS 3 a été certifiée conformément aux normes de sécurité

en vigueur au Canada, en Europe et aux Etats-Unis. Merci de vous

reporter aux indications mentionnées sur le panneau arrière de

l’instrument ainsi qu’au document de Déclaration de Conformité aux

normes pour lesquelles l’instrument a été déclaré conforme.

Capot de protection

Un capot de protection est installé sur

chaque tête de pompe.

Il protège l’utilisateur des risques

mécaniques présents dès lors que la tête

de pompe tourne.

Ne pas faire fonctionner la pompe sans

son capot de protection.

Figure 2

Tête de pompe

R2 équipée de

son capot de

protection

7

MINIPULS® 3 PERISTALTIC PUMP | USER'S GUIDE

CAPOT DE PROTECTION

Conditions de fonctionnement

L’accès au panneau arrière doit être libre car l’instrument doit pouvoir

être déconnecté de sa source d’alimentation avant toute opération

d’entretien, de réparation ou de remplacement de pièces.

Ne faîtes fonctionner l’appareil qu’en utilisant le bloc d’alimentation

fourni et uniquement à la tension indiquée sur l’étiquette située à

l’arrière de l’instrument.

Solvants

Respectez les Bonnes Pratiques de Laboratoire lors de la

manipulation de solvants. Si des liquides dangereux sont utilisés,

assurez-vous que la ventilation est adéquate et portez en

permanence un équipement de protection individuelle (EPI), tel que :

lunettes, gants et vêtements de protection.

Reportez-vous aux Fiches de Données de Sécurité pour les solvants

avant toute utilisation.

Pièces détachées

Assurez-vous de n’utiliser exclusivement que les pièces détachées

préconisées dans ce guide. Ne tentez pas de réparer ou remplacer

des pièces ne figurant pas dans ce guide.

Si le remplacement de pièces ne figurant pas dans ce guide s’avérait

nécessaire, merci de contacter votre représentant Gilson local.

8

SOLVANTS | MINIPULS® 3 PERISTALTIC PUMP

SOLVANTS

Chapter 1

CHAPTER 1 | INTRODUCTION

Gilson’s MINIPULS® 3 Peristaltic Pump was specifically designed

to meet process laboratory liquid handling needs. The MINIPULS 3

combines microprocessor speed control with a high-torque stepper

motor. Chemical-resistant pump heads, equipped with five or ten

stainless steel rollers, set the performance standard in producing

smooth, low-pulse flow and reproducible flow rates at higher

pressures.

This user’s guide describes how to set up and operate a MINIPULS 3.

It also describes some of the methodology required to obtain

accurate reproducible results.

IN THIS CHAPTER

• Unpacking on page 10

• Customer Service on page 10

• Description on page 11

• Speed Control Module on page 12

• Pump Head with Safety Cover on page 15

9

MINIPULS® 3 PERISTALTIC PUMP | USER'S GUIDE

Unpacking

Upon receipt of your MINIPULS 3, unpack it and check that all of the

parts are included even if it is not for immediate use. Report any loss

or damage immediately. Keep the original packaging in case the

MINIPULS 3 must be returned to the factory.

After unpacking the box, you should have the following:

• speed control module

• standard accessory package

• external power supply

• documentation

A pump head is required, but ordered separately.

Customer Service

Gilson, Inc. and its worldwide network of authorized representatives

provide customers with the following types of assistance: sales,

technical support, applications, and instrument repair.

If you need assistance, please contact your local Gilson

representative. Specific contact information can be found at www.

gilson.com. To help us serve you quickly and efficiently, please refer

to Repair and Return Policies on page 50.

10

UNPACKING | MINIPULS® 3 PERISTALTIC PUMP

UNPACKING

Description

Gilson’s MINIPULS 3 is a peristaltic pump, designed for transferring

fluids with a high level of speed stability and a low pulsation level. It

has many applications, including the following:

• transferring solutions, emulsions, suspensions, and gases at up

to 200°C.

• pumping liquids through chromatographic systems against a

back pressure of up to 0.5 MPa (72.5 psi) when controlled by a

Gilson fraction collector, for example.

• automation of biological analyses by proportionally mixing a

sample with several reagents (flowinjection analysis).

• continuously sampling the components of a production process

(reactors, fermenters, etc.).

• formation of gradients (concentration, pH, etc.).

Control of the MINIPULS 3 is from a computer via GSIOC and Gilson

TRILUTION® LH software, remote control by contact closure, or

manual control by front panel operation.

11

MINIPULS® 3 PERISTALTIC PUMP | USER'S GUIDE

DESCRIPTION

Speed Control Module

The figure shows a general view of a MINIPULS 3, before the head is

installed.

Front Panel

Display

Keypad

Figure 3

Front Panel

12

SPEED CONTROL MODULE | MINIPULS® 3 PERISTALTIC PUMP

SPEED CONTROL MODULE

The front panel consists of:

• a keypad

• Slower - Decrease the pumpspeed

• Faster - Increase the pumpspeed

• Rabbit - Set speed to 48 rpm for priming

• Forwards - Start the pump clockwise

• Backwards - Start the pump counter-clockwise

• Stop - Stop the pump

• a display

13

MINIPULS® 3 PERISTALTIC PUMP | USER'S GUIDE

SPEED CONTROL MODULE

Rear Panel

GSIOC

Fan

Power

on/o

switch

Contact

input port

DC

input

USB

device

Figure 4

Rear Panel

The rear panel consists of:

• a power on/off switch

• a DC input

• a fan

• a contact input port

• a 9-pin GSIOC port

• a USB device port (for service use only)

14

SPEED CONTROL MODULE | MINIPULS® 3 PERISTALTIC PUMP

SPEED CONTROL MODULE

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